laboratory experiments for chemistry textbook

Laboratory Manual: General Chemistry I Honors - First Edition

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Adedoyin M. Adeyiga, Cheyney University of Pennsylvania

Publisher: The Pennsylvania Alliance for Design of Open Textbooks (PA-ADOPT)

Language: English

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Calculations In the Chemistry Laboratory
Experiment One: Which Antacid is Most Effective?
Experiment Two: Extraction of Fat and Determination of Fat Content of Candy Bars
Experiment Three: Identifying Some Constituents of Bones
Experiment Four: Synthesis of Tylenol
Experment Five: Separation and Identification of Components of Combination Analgesics

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About the book.

General Chemistry I Honors Laboratory Manual (2023) is an eTextbook designed to provide a practical, hands-on approach to learning chemistry for students taking General Chemistry I Honors courses. The manual covers fundamental principles of chemistry, including atomic structure, chemical bonding, stoichiometry, gas laws, and thermodynamics. The book is divided into chapters, each focusing on a specific topic. Each experiment in the manual is accompanied by step-by-step instructions, pre-lab questions, and post-lab questions, helping students to develop their analytical and problem-solving skills.

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Dr. Adedoyin M. Adeyiga , Cheyney University of Pennsylvania

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Comprehensive Organic Chemistry Experiments for the Laboratory Classroom

This expansive and practical textbook contains organic chemistry experiments for teaching in the laboratory at the undergraduate level covering a range of functional group transformations and key organic reactions.The editorial team have collected contributions from around the world and standardized them for publication. Each experiment will explore a modern chemistry scenario, such as: sustainable chemistry; application in the pharmaceutical industry; catalysis and material sciences, to name a few. All the experiments will be complemented with a set of questions to challenge the students and a section for the instructors, concerning the results obtained and advice on getting the best outcome from the experiment. A section covering practical aspects with tips and advice for the instructors, together with the results obtained in the laboratory by students, has been compiled for each experiment.

Targeted at professors and lecturers in chemistry, this useful text will provide up to date experiments putting the science into context for the students.

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Comprehensive Organic Chemistry Experiments for the Laboratory Classroom, The Royal Society of Chemistry, 2016.

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Front Matter
1.1. Separation, Purification and Identification of the Components of a Mixture p1-5 By Abel J. S. C. Vieira ; Abel J. S. C. Vieira Faculty of Sciences and Technology, Universidade Nova de Lisboa 2829-516 Caparica Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Elvira M. S. M. Gaspar Elvira M. S. M. Gaspar Faculty of Sciences and Technology, Universidade Nova de Lisboa 2829-516 Caparica Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 1.1. Separation, Purification and Identification of the Components of a Mixture in another window
1.2. Isolation of (+)-Limonene from Orange Oil p6-8 By João P. Telo João P. Telo Centro de Química Estrutural, Instituto Superior Técnico, Universidade de Lisboa Av. Rovisco Pais 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 1.2. Isolation of (+)-Limonene from Orange Oil in another window
1.3. Isolation of Plant Pigments from Green and Red Leaves p9-13 By Alice M. Dias ; Alice M. Dias Department of Chemistry, University of Minho Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria La S. Ferreira Maria La S. Ferreira Department of Chemistry, University of Minho Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 1.3. Isolation of Plant Pigments from Green and Red Leaves in another window
1.4. Extraction of Usnic Acid from Lichen p14-17 By Dietmar K. Kennepohl Dietmar K. Kennepohl Athabasca University 1 University Drive Athabasca Alberta T9S 3A3 Canada [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 1.4. Extraction of Usnic Acid from Lichen in another window
1.5. Thin-Layer Chromatography of Plants Pigments p18-22 By Ana Margarida Madureira ; Ana Margarida Madureira iMed.ULisboa, Faculty of Pharmacy, University of Lisbon Av. Professor Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria-José U. Ferreira Maria-José U. Ferreira iMed.ULisboa, Faculty of Pharmacy, University of Lisbon Av. Professor Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 1.5. Thin-Layer Chromatography of Plants Pigments in another window
1.6. Isolation of Cinnamaldehyde from Cinnamon p23-25 By Raquel F. M. Frade ; Raquel F. M. Frade iMed.ULisboa, Faculdade de Farmácia da Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Dulce Simão ; Dulce Simão Department of Chemical Engineering, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso iMed.ULisboa, Faculdade de Farmácia da Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 1.6. Isolation of Cinnamaldehyde from Cinnamon in another window
1.7. Isolation and Structural Identification of Piperine, the Major Alkaloid of Black Pepper p26-29 By Andreia Mónico ; Andreia Mónico iMed.ULisboa, Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Angela Paterna ; Angela Paterna iMed.ULisboa, Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Mariana A. Reis ; Mariana A. Reis iMed.ULisboa, Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ricardo Ferreira ; Ricardo Ferreira iMed.ULisboa, Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Noélia Duarte ; Noélia Duarte iMed.ULisboa, Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana M. Madureira ; Ana M. Madureira iMed.ULisboa, Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria-José U. Ferreira Maria-José U. Ferreira iMed.ULisboa, Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 1.7. Isolation and Structural Identification of Piperine, the Major Alkaloid of Black Pepper in another window
1.8. Caffeine Extraction from Tea and Coffee p30-34 By Ana Margarida Madureira ; Ana Margarida Madureira iMed.ULisboa, Faculty of Pharmacy, University of Lisbon Av. Professor Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Abel J. S. C. Vieira ; Abel J. S. C. Vieira Faculty of Sciences and Technology, Universidade Nova de Lisboa, Campus de Caparica 2829-516 Caparica, Caparica Portugal Search for other works by this author on: This Site PubMed Google Scholar Maria-José U. Ferreira Maria-José U. Ferreira iMed.ULisboa, Faculty of Pharmacy, University of Lisbon Av. Professor Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 1.8. Caffeine Extraction from Tea and Coffee in another window
1.9. Isolation of the Alkaloid Lupanine from Lupinus albus Seeds p35-37 By Ana M. Lourenço ; Ana M. Lourenço REQUIMTE, Departamento de Química, Faculdade de Ciências e Tecnologia, Universidade Nova de Lisboa 2829-516 Caparica Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Luísa Maria Ferreira Luísa Maria Ferreira REQUIMTE, Departamento de Química, Faculdade de Ciências e Tecnologia, Universidade Nova de Lisboa 2829-516 Caparica Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 1.9. Isolation of the Alkaloid Lupanine from Lupinus albus Seeds in another window
1.10. Isolation and Purification of Atropine, a Tropane Alkaloid Obtained from Atropa belladonna L. (Solanaceae) p38-42 By Gustavo da Silva Gustavo da Silva Department of Pharmacological Sciences, Research Institute for Medicines and Pharmaceutical Sciences (iMed.ULisboa), Faculty of Pharmacy – University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 1.10. Isolation and Purification of Atropine, a Tropane Alkaloid Obtained from Atropa belladonna L. (Solanaceae) in another window
1.11. Isolation and Purification of Carnosol from Salvia officinalis † p43-45 By Filipe Pereira ; Filipe Pereira Universidade Lusófona Research Center for Biosciences & Health Technologies (CBIOS) Campo Grande 376 1749-024 Lisboa Portugal Search for other works by this author on: This Site PubMed Google Scholar Patrícia Rijo Patrícia Rijo Universidade Lusófona Research Center for Biosciences & Health Technologies (CBIOS) Campo Grande 376 1749-024 Lisboa Portugal Instituto de Investigação do Medicamento (iMed.ULisboa), Faculdade de Farmácia da Universidade de Lisboa Av. Professor Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 1.11. Isolation and Purification of Carnosol from Salvia officinalis<a href="javascript:;" reveal-id="BK9781849739634-00043-fn1" data-open="BK9781849739634-00043-fn1" class="link link-ref link-reveal xref-fn js-xref-fn split-view-modal">†</a> in another window
1.12. Analysis of Racemic and ( S )-Ibuprofen p46-50 By C. Fernandes ; C. Fernandes Laboratório de Química Orgânica e Farmacêutica, Departamento de Ciências Químicas, Faculdade de Farmácia, Universidade do Porto Portugal Centro Interdisciplinar de Investigação Marinha e Ambiental (CIIMAR/CIMAR), Universidade do Porto Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar H. Cidade ; H. Cidade Laboratório de Química Orgânica e Farmacêutica, Departamento de Ciências Químicas, Faculdade de Farmácia, Universidade do Porto Portugal Centro Interdisciplinar de Investigação Marinha e Ambiental (CIIMAR/CIMAR), Universidade do Porto Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar S. Cravo ; S. Cravo Laboratório de Química Orgânica e Farmacêutica, Departamento de Ciências Químicas, Faculdade de Farmácia, Universidade do Porto Portugal Search for other works by this author on: This Site PubMed Google Scholar E. Sousa ; E. Sousa Laboratório de Química Orgânica e Farmacêutica, Departamento de Ciências Químicas, Faculdade de Farmácia, Universidade do Porto Portugal Centro Interdisciplinar de Investigação Marinha e Ambiental (CIIMAR/CIMAR), Universidade do Porto Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Pinto M. Pinto Laboratório de Química Orgânica e Farmacêutica, Departamento de Ciências Químicas, Faculdade de Farmácia, Universidade do Porto Portugal Centro Interdisciplinar de Investigação Marinha e Ambiental (CIIMAR/CIMAR), Universidade do Porto Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 1.12. Analysis of Racemic and (S)-Ibuprofen in another window
1.13. Determining Partition Coefficients of Sulfonamides by Reversed-Phase Chromatography p51-55 By E. Sousa ; E. Sousa Laboratório de Química Orgânica e Farmacêutica, Departamento de Ciências Químicas, Faculdade de Farmácia, Universidade do Porto Portugal Centro Interdisciplinar de Investigação Marinha e Ambiental (CIIMAR/CIMAR), Universidade do Porto Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar S. Cravo ; S. Cravo Laboratório de Química Orgânica e Farmacêutica, Departamento de Ciências Químicas, Faculdade de Farmácia, Universidade do Porto Portugal Search for other works by this author on: This Site PubMed Google Scholar C. Fernandes ; C. Fernandes Laboratório de Química Orgânica e Farmacêutica, Departamento de Ciências Químicas, Faculdade de Farmácia, Universidade do Porto Portugal Centro Interdisciplinar de Investigação Marinha e Ambiental (CIIMAR/CIMAR), Universidade do Porto Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Pinto M. Pinto Laboratório de Química Orgânica e Farmacêutica, Departamento de Ciências Químicas, Faculdade de Farmácia, Universidade do Porto Portugal Centro Interdisciplinar de Investigação Marinha e Ambiental (CIIMAR/CIMAR), Universidade do Porto Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 1.13. Determining Partition Coefficients of Sulfonamides by Reversed-Phase Chromatography in another window
2.1.1. A S N 1 Reaction: Synthesis of tert -Butyl Chloride p56-60 By Emília Valente ; Emília Valente Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisbon Portugal Search for other works by this author on: This Site PubMed Google Scholar Catarina Dias ; Catarina Dias Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisbon Portugal Search for other works by this author on: This Site PubMed Google Scholar Luís Constantino Luís Constantino Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisbon Portugal Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Professor Gama Pinto 1649-003 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.1.1. A SN1 Reaction: Synthesis of tert-Butyl Chloride in another window
2.1.2. Optimizing the Reaction Conditions for the Synthesis of tert -Pentyl Chloride p61-63 By Jane Brock Greco Jane Brock Greco Department of Chemistry, Johns Hopkins University 3400 N. Charles St. Baltimore MD 21218 USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.1.2. Optimizing the Reaction Conditions for the Synthesis of tert-Pentyl Chloride in another window
2.1.3. Kinetics of a S N 1 Reaction p64-67 By Paulo Coelho ; Paulo Coelho Centro de Química – Vila Real, Universidade de Trás-os-Montes e Alto Douro 5001-801 Vila Real Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Céu Sousa Céu Sousa Centro de Química – Vila Real, Universidade de Trás-os-Montes e Alto Douro 5001-801 Vila Real Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.1.3. Kinetics of a SN1 Reaction in another window
2.1.4. Counterion Effects in the Nucleophilic Substitution Reaction of the Acetate Ion with Alkyl Bromides in the Synthesis of Esters p68-71 By Ingrid Montes ; Ingrid Montes Department of Chemistry, University of Puerto Rico-Río Piedras Campus PO Box 23346 San Juan PR 00931-3346 Puerto Rico USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Elizabeth Valentín ; M. Elizabeth Valentín Department of Chemistry, University of Puerto Rico-Río Piedras Campus PO Box 23346 San Juan PR 00931-3346 Puerto Rico USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar Waldemar Adam Waldemar Adam Department of Chemistry, University of Puerto Rico-Río Piedras Campus PO Box 23346 San Juan PR 00931-3346 Puerto Rico USA [email protected] Institute of Organic Chemistry, University of Wuerzburg Am Hubland D-97094 Wuerzburg Germany Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.1.4. Counterion Effects in the Nucleophilic Substitution Reaction of the Acetate Ion with Alkyl Bromides in the Synthesis of Esters in another window
2.1.5. N -Alkylation of Pyrazole: Reaction in an Ionic Liquid p72-75 By Clarissa P. Frizzo ; Clarissa P. Frizzo Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Marcos A. P. Martins ; Marcos A. P. Martins Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Caroline R. Bender ; Caroline R. Bender Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Paulo R. S. Salbego ; Paulo R. S. Salbego Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Aniele Z. Tier ; Aniele Z. Tier Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Geórgia C. Zimmer ; Geórgia C. Zimmer Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Guilherme C. Paveglio ; Guilherme C. Paveglio Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Helio G. Bonacorso Helio G. Bonacorso Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.1.5. N-Alkylation of Pyrazole: Reaction in an Ionic Liquid in another window
2.1.6. Conversion of Alcohols into Alkyl Chlorides Using Cyanuric Chloride p76-79 By Eliana Martins ; Eliana Martins Instituto de Investigação do Medicamento (iMed.ULisboa), Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Catarina A. B. Rodrigues ; Catarina A. B. Rodrigues Instituto de Investigação do Medicamento (iMed.ULisboa), Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso Instituto de Investigação do Medicamento (iMed.ULisboa), Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.1.6. Conversion of Alcohols into Alkyl Chlorides Using Cyanuric Chloride in another window
2.1.7. Synthesis of Phenacetin p80-83 By Paulo Coelho ; Paulo Coelho Centro de Química – Vila Real, Universidade de Trás-os-Montes e Alto Douro 5001-801 Vila Real Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Céu Sousa Céu Sousa Centro de Química – Vila Real, Universidade de Trás-os-Montes e Alto Douro 5001-801 Vila Real Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.1.7. Synthesis of Phenacetin in another window
2.1.8. One-Step Synthesis of 4(3 H )-Quinazolinones: An Important Heterocyclic Scaffold in Medicinal Chemistry p84-86 By André Dias ; André Dias Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Professor Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Rui Moreira ; Rui Moreira Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Professor Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana S. Ressurreição Ana S. Ressurreição Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Professor Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.1.8. One-Step Synthesis of 4(3H)-Quinazolinones: An Important Heterocyclic Scaffold in Medicinal Chemistry in another window
2.1.9. Controlled Monoalkylation of the Structurally Rigid Bicyclic System Isomannide p87-91 By M. Manuela ; M. Manuela REQUIMTE, Chemistry Department, Faculdade de Ciências e Tecnologia, Universidade Nova de Lisboa 2827-516 Caparica Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar A. Pereira A. Pereira REQUIMTE, Chemistry Department, Faculdade de Ciências e Tecnologia, Universidade Nova de Lisboa 2827-516 Caparica Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.1.9. Controlled Monoalkylation of the Structurally Rigid Bicyclic System Isomannide in another window
2.1.10. Regioselective N -alkylation of Adenine by Nucleophilic Substitution p92-94 By Ana I. Vicente ; Ana I. Vicente iMed.ULisboa, Faculdade de Farmácia da Universidade de Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso iMed.ULisboa, Faculdade de Farmácia da Universidade de Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.1.10. Regioselective N-alkylation of Adenine by Nucleophilic Substitution in another window
2.1.11. Gabriel Synthesis of n -Octylamine Under Phase-Transfer Catalysis: The First Step p95-98 By Renata Riva ; Renata Riva Search for other works by this author on: This Site PubMed Google Scholar Luca Banfi Luca Banfi Dipartimento di Chimica e Chimica Industriale Via Dodecaneso 31 16146 Genova Italy [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.1.11. Gabriel Synthesis of n-Octylamine Under Phase-Transfer Catalysis: The First Step in another window
2.1.12. Preparation of Diethyl 2,3- O -isopropylidene- l -tartrate p99-102 By Naylil M. R. Capreti ; Naylil M. R. Capreti Institute of Chemistry, State University of Campinas (Unicamp) C.P. 6154 13083-970 Campinas SP Brazil [email protected] Search for other works by this author on: This Site PubMed Google Scholar Igor D. Jurberg Igor D. Jurberg Institute of Chemistry, State University of Campinas (Unicamp) C.P. 6154 13083-970 Campinas SP Brazil [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.1.12. Preparation of Diethyl 2,3-O-isopropylidene-l-tartrate in another window
2.1.13. Redox-Neutral Synthesis of a Cyclic N , O -Acetal from Salicylaldehyde and 1,2,3,4-Tetrahydroisoquinoline p103-106 By Claire L. Jarvis ; Claire L. Jarvis Rutgers, the State University of New Jersey, Department of Chemistry and Chemical Biology, Rutgers University 610 Taylor Road Piscataway NJ 08854-8087 USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar Daniel Seidel Daniel Seidel Rutgers, the State University of New Jersey, Department of Chemistry and Chemical Biology, Rutgers University 610 Taylor Road Piscataway NJ 08854-8087 USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.1.13. Redox-Neutral Synthesis of a Cyclic N,O-Acetal from Salicylaldehyde and 1,2,3,4-Tetrahydroisoquinoline in another window
2.2.1. Selective C -acylation of 3-Methyl-1-phenyl-pyrazol-5-one p107-111 By Vanya B. Kurteva ; Vanya B. Kurteva Institute of Organic Chemistry with Centre of Phytochemistry, Bulgarian Academy of Sciences Acad. G. Bonchev str., bl. 9 1113 Sofia Bulgaria [email protected] Search for other works by this author on: This Site PubMed Google Scholar Lubomir A. Lubenov ; Lubomir A. Lubenov Institute of Organic Chemistry with Centre of Phytochemistry, Bulgarian Academy of Sciences Acad. G. Bonchev str., bl. 9 1113 Sofia Bulgaria [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria A. Petrova Maria A. Petrova University of Chemical Technology and Metallurgy, Department of General and Inorganic Chemistry 8 Kliment Ohridski blvd. 1756 Sofia Bulgaria Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.2.1. Selective C-acylation of 3-Methyl-1-phenyl-pyrazol-5-one in another window
2.2.2. Organocatalytic Asymmetric α-Arylation of Aldehydes p112-116 By Mette Overgaard ; Mette Overgaard Department of Chemistry, Aarhus University DK-8000 Aarhus C Denmark [email protected] Search for other works by this author on: This Site PubMed Google Scholar Pernille H. Poulsen ; Pernille H. Poulsen Department of Chemistry, Aarhus University DK-8000 Aarhus C Denmark [email protected] Search for other works by this author on: This Site PubMed Google Scholar Karl Anker Jørgensen Karl Anker Jørgensen Department of Chemistry, Aarhus University DK-8000 Aarhus C Denmark [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.2.2. Organocatalytic Asymmetric α-Arylation of Aldehydes in another window
2.2.3. Matteson Homologation of Pinacol Boronic Ester: An Efficient Method Using the Boronate Complexes p117-119 By Sébastien Balieu ; Sébastien Balieu Université de Rouen, IRCOF 1 Rue Tesnières - 76130 Mont Saint Aignan France [email protected] Search for other works by this author on: This Site PubMed Google Scholar Asmaa Bouyahya ; Asmaa Bouyahya Université de Rouen, IRCOF 1 Rue Tesnières - 76130 Mont Saint Aignan France [email protected] Search for other works by this author on: This Site PubMed Google Scholar Jean-Philippe Bouillon Jean-Philippe Bouillon Université de Rouen, IRCOF 1 Rue Tesnières - 76130 Mont Saint Aignan France [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.2.3. Matteson Homologation of Pinacol Boronic Ester: An Efficient Method Using the Boronate Complexes in another window
2.2.4. A Practical Organocatalytic Alkylation Reaction with Benzodithiolylium Tetrafluoroborate p120-124 By Pier Giorgio Cozzi ; Pier Giorgio Cozzi Alma Mater Studiorum – Università di Bologna, Dipartimento di Chimica “G. Ciamician” Via Selmi 2 40126 Bologna Italy [email protected] Search for other works by this author on: This Site PubMed Google Scholar Marco Bandini ; Marco Bandini Alma Mater Studiorum – Università di Bologna, Dipartimento di Chimica “G. Ciamician” Via Selmi 2 40126 Bologna Italy [email protected] Search for other works by this author on: This Site PubMed Google Scholar Andrea Gualandi ; Andrea Gualandi Alma Mater Studiorum – Università di Bologna, Dipartimento di Chimica “G. Ciamician” Via Selmi 2 40126 Bologna Italy [email protected] Search for other works by this author on: This Site PubMed Google Scholar Luca Mengozzi Luca Mengozzi Alma Mater Studiorum – Università di Bologna, Dipartimento di Chimica “G. Ciamician” Via Selmi 2 40126 Bologna Italy [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.2.4. A Practical Organocatalytic Alkylation Reaction with Benzodithiolylium Tetrafluoroborate in another window
2.2.5. Oxazolidinone Mediated Enantioselective Allylation p125-128 By Jonathan D. Sellars ; Jonathan D. Sellars Chemistry Department, University of Durham South Road Durham DH1 3LE UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar AnnMarie C. O’Donoghue ; AnnMarie C. O’Donoghue Chemistry Department, University of Durham South Road Durham DH1 3LE UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ian R. Baxendale ; Ian R. Baxendale Chemistry Department, University of Durham South Road Durham DH1 3LE UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar John M. Sanderson ; John M. Sanderson Chemistry Department, University of Durham South Road Durham DH1 3LE UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Elizabeth J. Grayson Elizabeth J. Grayson Chemistry Department, University of Durham South Road Durham DH1 3LE UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 2.2.5. Oxazolidinone Mediated Enantioselective Allylation in another window
3.1.1. Synthesis of Paracetamol by Acetylation p129-132 By Catarina Dias ; Catarina Dias Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal Search for other works by this author on: This Site PubMed Google Scholar Emília Valente ; Emília Valente Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal Search for other works by this author on: This Site PubMed Google Scholar Luís Constantino Luís Constantino Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.1. Synthesis of Paracetamol by Acetylation in another window
3.1.2. Synthesis and Characterization of N , N ′-Dicyclohexyl- N , N ′-dimethyl-propan-1,3-diamide p133-135 By Ana Paula Paiva ; Ana Paula Paiva Centro de Química e Bioquímica, Departamento de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa Rua Ernesto de Vasconcelos, C8, Campo Grande 1749-016 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Osvaldo Ortet Osvaldo Ortet Centro de Química e Bioquímica, Departamento de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa Rua Ernesto de Vasconcelos, C8, Campo Grande 1749-016 Lisbon Portugal [email protected] Departamento de Ciência e Tecnologia, Universidade de Cabo Verde 379C Praia Santiago Island Cape Verde Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.2. Synthesis and Characterization of N,N′-Dicyclohexyl-N,N′-dimethyl-propan-1,3-diamide in another window
3.1.3. Synthesis and Characterisation of an Ester from 4-Nitrobenzoyl Chloride p136-138 By Iain A. Smellie ; Iain A. Smellie School of Chemistry, University of St Andrews North Haugh, St Andrews Fife KY16 9ST UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Matt L. Clarke ; Matt L. Clarke School of Chemistry, University of St Andrews North Haugh, St Andrews Fife KY16 9ST UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Leanne Harris ; Leanne Harris School of Chemistry, University of St Andrews North Haugh, St Andrews Fife KY16 9ST UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Andrew. J. Miller Andrew. J. Miller School of Chemistry, University of St Andrews North Haugh, St Andrews Fife KY16 9ST UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.3. Synthesis and Characterisation of an Ester from 4-Nitrobenzoyl Chloride in another window
3.1.4. Green Esterification: The Synthesis of Aromas in the Presence of an Acid Resin p139-141 By José E. Castanheiro ; José E. Castanheiro Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora Rua Romão Ramalho, no. 59 7000-671 Évora Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar António P. S. Teixeira ; António P. S. Teixeira Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora Rua Romão Ramalho, no. 59 7000-671 Évora Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar António M. D. R. L. Pereira António M. D. R. L. Pereira Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora Rua Romão Ramalho, no. 59 7000-671 Évora Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.4. Green Esterification: The Synthesis of Aromas in the Presence of an Acid Resin in another window
3.1.5. Acetylation of Cholesterol and Purification by Column Chromatography p142-146 By Emília Valente ; Emília Valente Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisbon Portugal Search for other works by this author on: This Site PubMed Google Scholar Catarina Dias ; Catarina Dias Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisbon Portugal Search for other works by this author on: This Site PubMed Google Scholar Luís Constantino Luís Constantino Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisbon Portugal Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.5. Acetylation of Cholesterol and Purification by Column Chromatography in another window
3.1.6. Synthesis of Hippuric Acid: An Example of Amide Bond Formation p147-150 By Ana S. Ressurreição ; Ana S. Ressurreição Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Professor Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria de Jesus Perry ; Maria de Jesus Perry Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Professor Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana Paula Francisco ; Ana Paula Francisco Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Professor Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Francisca Lopes Francisca Lopes Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Professor Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.6. Synthesis of Hippuric Acid: An Example of Amide Bond Formation in another window
3.1.7. Preparation of a Sulfathiazole Prodrug via N -acylation with Succinic Anhydride p151-153 By Pedro M. P. Gois ; Pedro M. P. Gois Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Francisca Lopes ; Francisca Lopes Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Alexandre F. Trindade Alexandre F. Trindade Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.7. Preparation of a Sulfathiazole Prodrug via N-acylation with Succinic Anhydride in another window
3.1.8. Determination of the Absolute Configuration of Enantioenriched Secondary Alcohols via Thin-Layer Chromatography p154-158 By Alexander J. Wagner ; Alexander J. Wagner Department of Chemistry, University of California–Irvine 1102 Natural Sciences II Irvine CA 92697 USA [email protected] [email protected] [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Shawn M. Miller ; Shawn M. Miller Department of Chemistry, University of California–Irvine 1102 Natural Sciences II Irvine CA 92697 USA [email protected] [email protected] [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Scott D. Rychnovsky ; Scott D. Rychnovsky Department of Chemistry, University of California–Irvine 1102 Natural Sciences II Irvine CA 92697 USA [email protected] [email protected] [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Renée D. Link Renée D. Link Department of Chemistry, University of California–Irvine 1102 Natural Sciences II Irvine CA 92697 USA [email protected] [email protected] [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.8. Determination of the Absolute Configuration of Enantioenriched Secondary Alcohols via Thin-Layer Chromatography in another window
3.1.9. Anhydride Aminolysis: Synthesis of N -arylmaleamic Acids p159-161 By Artur M. S. Silva ; Artur M. S. Silva Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Augusto C. Tomé ; Augusto C. Tomé Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Diana C. G. A. Pinto ; Diana C. G. A. Pinto Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernando Domingues ; Fernando Domingues Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Graça M. Oliveira Rocha ; Graça M. Oliveira Rocha Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar José A. S. Cavaleiro ; José A. S. Cavaleiro Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Graça P. M. S. Neves ; M. Graça P. M. S. Neves Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Amparo F. Faustino ; M. Amparo F. Faustino Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Mário M. Q. Simões Mário M. Q. Simões Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.9. Anhydride Aminolysis: Synthesis of N-arylmaleamic Acids in another window
3.1.10. Synthesis of N -arylmaleimides p162-164 By Artur M. S. Silva ; Artur M. S. Silva Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Augusto C. Tomé ; Augusto C. Tomé Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Diana C. G. A. Pinto ; Diana C. G. A. Pinto Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernando Domingues ; Fernando Domingues Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Graça M. Oliveira Rocha ; Graça M. Oliveira Rocha Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar José A. S. Cavaleiro ; José A. S. Cavaleiro Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Graça P. M. S. Neves ; M. Graça P. M. S. Neves Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Amparo F. Faustino ; M. Amparo F. Faustino Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Mário M. Q. Simões Mário M. Q. Simões Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.10. Synthesis of N-arylmaleimides in another window
3.1.11. Synthesis and Characterization of N -Cyclohexyl- N- methyloctanamide p165-168 By Ana Paula Paiva ; Ana Paula Paiva Centro de Química e Bioquímica, Departamento de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Osvaldo Ortet Osvaldo Ortet Centro de Química e Bioquímica, Departamento de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa Lisboa Portugal [email protected] Departamento de Ciência e Tecnologia, Universidade de Cabo Verde Praia Cape Verde Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.11. Synthesis and Characterization of N-Cyclohexyl-N-methyloctanamide in another window
3.1.12. Effect of a Catalyst in the Acylation of Alcohols with Acetic Anhydride: Manipulation of a Natural Aroma p169-171 By Mónica S. Estevão ; Mónica S. Estevão iMed.UL, Faculdade de Farmácia da Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso iMed.UL, Faculdade de Farmácia da Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.12. Effect of a Catalyst in the Acylation of Alcohols with Acetic Anhydride: Manipulation of a Natural Aroma in another window
3.1.13. Synthesis of 4,5-Dichloro-1,2-dicyanobenzene p172-174 By Dulce Simão Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.13. Synthesis of 4,5-Dichloro-1,2-dicyanobenzene in another window
3.1.14. Synthesis of N-tert -Butyloxycarbonyl-3-nitro- l -tyrosine Methyl Ester p175-177 By Susana P. G. Costa ; Susana P. G. Costa University of Minho, Department of Chemistry, Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Manuela M. Raposo ; M. Manuela M. Raposo University of Minho, Department of Chemistry, Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Cátia I. C. Esteves ; Cátia I. C. Esteves University of Minho, Department of Chemistry, Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar R. Cristina M. Ferreira R. Cristina M. Ferreira University of Minho, Department of Chemistry, Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.14. Synthesis of N-tert-Butyloxycarbonyl-3-nitro-l-tyrosine Methyl Ester in another window
3.1.15. Michael Addition Reaction Followed by Elimination Under Solvent-Free Conditions p178-181 By Marcos A. P. Martins ; Marcos A. P. Martins Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Clarissa P. Frizzo ; Clarissa P. Frizzo Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Aniele Z. Tier ; Aniele Z. Tier Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Guilherme C. Paveglio ; Guilherme C. Paveglio Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Caroline R. Bender ; Caroline R. Bender Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Paulo R. S. Salbego ; Paulo R. S. Salbego Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Geórgia C. Zimmer ; Geórgia C. Zimmer Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Nilo Zanatta Nilo Zanatta Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.15. Michael Addition Reaction Followed by Elimination Under Solvent-Free Conditions in another window
3.1.16. Synthesis of a γ-Keto-amide Derived from Thiophene Using a Carboxyl Ester as Precursor p182-187 By M. Manuela M. Raposo M. Manuela M. Raposo Department of Chemistry, University of Minho, Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.16. Synthesis of a γ-Keto-amide Derived from Thiophene Using a Carboxyl Ester as Precursor in another window
3.1.17. Cyclic Acetals for Regioselective Protection in Carbohydrate Synthesis: A Comparative Experiment p188-193 By Ana M. Matos ; Ana M. Matos Centro de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa C8, Piso 5, Campo Grande 1749-016 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Rafael Nunes ; Rafael Nunes Centro de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa C8, Piso 5, Campo Grande 1749-016 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Catarina Dias ; Catarina Dias Centro de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa C8, Piso 5, Campo Grande 1749-016 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Amélia P. Rauter Amélia P. Rauter Centro de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa C8, Piso 5, Campo Grande 1749-016 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.17. Cyclic Acetals for Regioselective Protection in Carbohydrate Synthesis: A Comparative Experiment in another window
3.1.18. Direct Diastereoselective Synthesis of the Tetrahydro-thiazolo[2,3- b ]isoindole Tricyclic Ring System p194-197 By Maria I. L. Soares ; Maria I. L. Soares Department of Chemistry, University of Coimbra Rua Larga 3004-535 Coimbra Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana Lúcia Cardoso ; Ana Lúcia Cardoso Department of Chemistry, University of Coimbra Rua Larga 3004-535 Coimbra Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Susana M. M. Lopes ; Susana M. M. Lopes Department of Chemistry, University of Coimbra Rua Larga 3004-535 Coimbra Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Teresa M. V. D. Pinho e Melo Teresa M. V. D. Pinho e Melo Department of Chemistry, University of Coimbra Rua Larga 3004-535 Coimbra Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.18. Direct Diastereoselective Synthesis of the Tetrahydro-thiazolo[2,3-b]isoindole Tricyclic Ring System in another window
3.1.19. Asymmetric Cyclocondensation Reaction Induced by Chiral Aminoalcohol p198-201 By Jorge Dourado ; Jorge Dourado Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria Pérez ; Maria Pérez Laboratory of Organic Chemistry, Faculty of Pharmacy and Institute of Biomedicine (IBUB), University of Barcelona Av. Joan XXIII, s/n 08028 Barcelona Spain Search for other works by this author on: This Site PubMed Google Scholar Rosa Griera ; Rosa Griera Laboratory of Organic Chemistry, Faculty of Pharmacy and Institute of Biomedicine (IBUB), University of Barcelona Av. Joan XXIII, s/n 08028 Barcelona Spain Search for other works by this author on: This Site PubMed Google Scholar Maria M. M. Santos Maria M. M. Santos Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.19. Asymmetric Cyclocondensation Reaction Induced by Chiral Aminoalcohol in another window
3.1.20. Synthesis and Characterization of Biodiesel Propyl Esters to Determine the Fatty Acid Content of Unknown Plant Oils p202-205 By Heidi R. Vollmer-Snarr ; Heidi R. Vollmer-Snarr Department of Chemistry, Stanford University S.G. Mudd Bldg., 333 Campus Drive Stanford CA 94305-4401 USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar Patrick A. Fracisco ; Patrick A. Fracisco Department of Chemistry, Stanford University S.G. Mudd Bldg., 333 Campus Drive Stanford CA 94305-4401 USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar Naiian Saephanh Naiian Saephanh Department of Chemistry, Stanford University S.G. Mudd Bldg., 333 Campus Drive Stanford CA 94305-4401 USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.1.20. Synthesis and Characterization of Biodiesel Propyl Esters to Determine the Fatty Acid Content of Unknown Plant Oils in another window
3.2.1. Synthesis of 7-Methoxy-4-oxo- N -phenyl-4 H -chromene-2-carboxamide p206-211 By Joana Reis ; Joana Reis Department of Chemistry and Biochemistry, Faculty of Sciences of University of Porto Rua do Campo Alegre s/n 4169-007 Porto Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Alexandra Gaspar ; Alexandra Gaspar Department of Chemistry and Biochemistry, Faculty of Sciences of University of Porto Rua do Campo Alegre s/n 4169-007 Porto Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernando Cagide ; Fernando Cagide Department of Chemistry and Biochemistry, Faculty of Sciences of University of Porto Rua do Campo Alegre s/n 4169-007 Porto Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernanda Borges Fernanda Borges Department of Chemistry and Biochemistry, Faculty of Sciences of University of Porto Rua do Campo Alegre s/n 4169-007 Porto Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.2.1. Synthesis of 7-Methoxy-4-oxo-N-phenyl-4H-chromene-2-carboxamide in another window
3.2.2. Synthesis of 2,3-Diphenylindenone p212-215 By João P. Telo João P. Telo Centro de Química Estrutural, Instituto Superior Técnico, Universidade de Lisboa Av. Rovisco Pais 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.2.2. Synthesis of 2,3-Diphenylindenone in another window
3.2.3. Synthesis of Dimedone p216-218 By Dulce Simão ; Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana C. Cerdeira Ana C. Cerdeira Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.2.3. Synthesis of Dimedone in another window
3.2.4. Acylation Reaction of Enol Ether Using an Ionic Liquid p219-222 By Marcos A. P. Martins ; Marcos A. P. Martins Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Clarissa P. Frizzo ; Clarissa P. Frizzo Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Geórgia C. Zimmer ; Geórgia C. Zimmer Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Caroline R. Bender ; Caroline R. Bender Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Paulo R. S. Salbego ; Paulo R. S. Salbego Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Aniele Z. Tier ; Aniele Z. Tier Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Nilo Zanatta Nilo Zanatta Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 3.2.4. Acylation Reaction of Enol Ether Using an Ionic Liquid in another window
4.1.1.1. Bromination of Cinnamic Acid p223-225 By Paulo Coelho ; Paulo Coelho Centro de, Química – Vila Real, Universidade de Trás-os-Montes e Alto Douro 5001-801 Vila Real Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Céu Sousa Céu Sousa Centro de, Química – Vila Real, Universidade de Trás-os-Montes e Alto Douro 5001-801 Vila Real Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.1.1. Bromination of Cinnamic Acid in another window
4.1.1.2. Preparation of Meso -1,2-Dibromo-1,2-diphenylethane p226-228 By Abel J. S. C. Vieira Abel J. S. C. Vieira Faculty of Sciences and Technology, Universidade Nova de Lisboa 2829-516 Caparica Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.1.2. Preparation of Meso-1,2-Dibromo-1,2-diphenylethane in another window
4.1.1.3. Bromination of ( E )-chalcones [( E )-1,3-Diarylprop-2-en-1-ones] p229-230 By Artur M. S. Silva ; Artur M. S. Silva Chemistry Department & QOPNA, University of Aveiro Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Augusto C. Tomé ; Augusto C. Tomé Chemistry Department & QOPNA, University of Aveiro Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Diana C. G. A. Pinto ; Diana C. G. A. Pinto Chemistry Department & QOPNA, University of Aveiro Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernando Domingues ; Fernando Domingues Chemistry Department & QOPNA, University of Aveiro Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Graça M. Oliveira Rocha ; Graça M. Oliveira Rocha Chemistry Department & QOPNA, University of Aveiro Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar José A. S. Cavaleiro ; José A. S. Cavaleiro Chemistry Department & QOPNA, University of Aveiro Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Graça P. M. S. Neves ; M. Graça P. M. S. Neves Chemistry Department & QOPNA, University of Aveiro Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Amparo F. Faustino ; M. Amparo F. Faustino Chemistry Department & QOPNA, University of Aveiro Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Mário M. Q. Simões Mário M. Q. Simões Chemistry Department & QOPNA, University of Aveiro Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.1.3. Bromination of (E)-chalcones [(E)-1,3-Diarylprop-2-en-1-ones] in another window
4.1.1.4. Preparation of trans -2-Bromocyclohexanol from Cyclohexanol p231-233 By Matheus P. Freitas Matheus P. Freitas Department of Chemistry, Federal University of Lavras 37200-000 Lavras MG Brazil [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.1.4. Preparation of trans-2-Bromocyclohexanol from Cyclohexanol in another window
4.1.1.5. Synthesis of trans -Cyclohexane-1,2-diol p234-236 By Dulce Simão ; Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana C. Cerdeira Ana C. Cerdeira Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.1.5. Synthesis of trans-Cyclohexane-1,2-diol in another window
4.1.1.6. Synthesis of Isobutylene and Its Use in Esterification Reactions p237-240 By Paula C. Castilho ; Paula C. Castilho Centro de Química da, Madeira, Universidade da Madeira, Campus Universitário da Penteada Piso 00 9020-105 Funchal Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Pedro Ideia ; Pedro Ideia Centro de Química da, Madeira, Universidade da Madeira, Campus Universitário da Penteada Piso 00 9020-105 Funchal Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Rúben Gonçalves Rúben Gonçalves Centro de Química da, Madeira, Universidade da Madeira, Campus Universitário da Penteada Piso 00 9020-105 Funchal Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.1.6. Synthesis of Isobutylene and Its Use in Esterification Reactions in another window
4.2.3.8. Synthesis of a Long-Wavelength Absorbing Squaraine Dye p396-398 By Paulo F. Santos ; Paulo F. Santos Departamento de Química and Centro de Química – Vila Real, Universidade de Trás-os-Montes e Alto Douro 5001-801 Vila Real Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Vânia C. Graça Vânia C. Graça Departamento de Química and Centro de Química – Vila Real, Universidade de Trás-os-Montes e Alto Douro 5001-801 Vila Real Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.3.8. Synthesis of a Long-Wavelength Absorbing Squaraine Dye in another window
4.2.3.9. Synthesis of π-Conjugated Systems Using Formylchromone as Building Block p399-402 By Carlos Fernandes ; Carlos Fernandes CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences of University of Porto Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Catarina Oliveira ; Catarina Oliveira CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences of University of Porto Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernanda Borges ; Fernanda Borges CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences of University of Porto Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Alexandra Gaspar Alexandra Gaspar CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences of University of Porto Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.3.9. Synthesis of π-Conjugated Systems Using Formylchromone as Building Block in another window
4.2.3.10. A Multi-Step Synthesis of Imidazolin-5-ones p403-407 By Gurunath Ramanathan ; Gurunath Ramanathan Indian Institute of Technology Kanpur Kanpur 208016 India [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ashish Singh Ashish Singh Indian Institute of Technology Kanpur Kanpur 208016 India [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.3.10. A Multi-Step Synthesis of Imidazolin-5-ones in another window
4.2.3.11. Baylis–Hillman Reaction Between 4-Nitrobenzaldehyde and Ethyl Acrylate p408-410 By Alexandre F. Trindade ; Alexandre F. Trindade Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar João Ravasco ; João Ravasco Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.3.11. Baylis–Hillman Reaction Between 4-Nitrobenzaldehyde and Ethyl Acrylate in another window
4.1.1.7. Hydroxyl Group Protection via Tetrahydropyranyl Ether Formation p241-243 By Ana I. B. Meirinhos ; Ana I. B. Meirinhos iMed.ULisboa Av. Professor Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Filipa Siopa ; Filipa Siopa iMed.ULisboa Av. Professor Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso iMed.ULisboa Av. Professor Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.1.7. Hydroxyl Group Protection via Tetrahydropyranyl Ether Formation in another window
4.1.1.8. Synthesis of (−)-Carvone from (+)-Limonene p244-246 By João P. Telo João P. Telo Centro de Química Estrutural, Instituto Superior Técnico, Universidade de Lisboa Av. Rovisco Pais 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.1.8. Synthesis of (−)-Carvone from (+)-Limonene in another window
4.2.3.12. Synthesis of Ethyl Mandelate Through a Rhodium-Catalysed Arylation Reaction with Ethyl Glyoxylate and Phenylboronic Acid p411-414 By Carolina S. Marques ; Carolina S. Marques University of Évora, Chemistry Department, School of Science and Technology, Centro de Química de Évora, Institute for Research and Advanced Training Rua Romão Ramalho, 59 7000-671 Évora Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Anthony J. Burke Anthony J. Burke University of Évora, Chemistry Department, School of Science and Technology, Centro de Química de Évora, Institute for Research and Advanced Training Rua Romão Ramalho, 59 7000-671 Évora Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.3.12. Synthesis of Ethyl Mandelate Through a Rhodium-Catalysed Arylation Reaction with Ethyl Glyoxylate and Phenylboronic Acid in another window
4.2.4.1. Preparation of Chalcone and Its Further Robinson Annulation with Ethyl Acetoacetate p420-423 By Nuno R. Candeias Nuno R. Candeias Department of Chemistry and Bioengineering, Tampere University of Technology Korkeakoulunkatu 8 Tampere FI-33101 Finland [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.4.1. Preparation of Chalcone and Its Further Robinson Annulation with Ethyl Acetoacetate in another window
4.1.1.9. Glycal Transformation into Surfactant 2-Deoxy Glycosides p247-251 By Catarina Dias ; Catarina Dias Centro de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa C8, Piso 5, Campo Grande 1749-016 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Amélia P. Rauter Amélia P. Rauter Centro de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa C8, Piso 5, Campo Grande 1749-016 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.1.9. Glycal Transformation into Surfactant 2-Deoxy Glycosides in another window
4.2.3.13. Enantioselective Synthesis and Derivatisation of 2-Hydroxy-1,2-diphenylethan-1-one p415-419 By Jonathan D. Sellars ; Jonathan D. Sellars Chemistry Department, University of Durham South Road Durham DH1 3LE UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar AnnMarie C. O’Donoghue ; AnnMarie C. O’Donoghue Chemistry Department, University of Durham South Road Durham DH1 3LE UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ian R. Baxendale ; Ian R. Baxendale Chemistry Department, University of Durham South Road Durham DH1 3LE UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar John M. Sanderson ; John M. Sanderson Chemistry Department, University of Durham South Road Durham DH1 3LE UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Elizabeth J. Grayson Elizabeth J. Grayson Chemistry Department, University of Durham South Road Durham DH1 3LE UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.3.13. Enantioselective Synthesis and Derivatisation of 2-Hydroxy-1,2-diphenylethan-1-one in another window
5.1.1. Synthesis of Methyl Orange p448-450 By Dulce Simão ; Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana C. Cerdeira Ana C. Cerdeira Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.1.1. Synthesis of Methyl Orange in another window
4.2.5.1. One-Pot Green Synthesis of Dihydropyran Heterocycles p428-431 By Dennis Russowsky ; Dennis Russowsky Laboratório de Síntese Organica K-210, Universidade Federal do Rio Grande do Sul, Instituto de Química Av. Bento Gonçalves, 9500 CEP 91501-970 Porto Alegre Rio Grande do Sul Brazil [email protected] Search for other works by this author on: This Site PubMed Google Scholar Camila S. Santos Camila S. Santos Laboratório de Síntese Organica K-210, Universidade Federal do Rio Grande do Sul, Instituto de Química Av. Bento Gonçalves, 9500 CEP 91501-970 Porto Alegre Rio Grande do Sul Brazil [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.5.1. One-Pot Green Synthesis of Dihydropyran Heterocycles in another window
4.2.5.2. Hantzsch Synthesis of Nifedipine p432-434 By Arno Kraft Arno Kraft Heriot-Watt University, Institute of Chemical Sciences, School of Engineering & Physical Sciences Riccarton Edinburgh EH14 4AS UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.5.2. Hantzsch Synthesis of Nifedipine in another window
4.1.1.10. Preparation of (1 R ,2 R ,3 R ,5 S )-(−)-Isopinocampheol Through a Hydroboration–Oxidation Reaction p252-256 By Marek P. Krzemiński Marek P. Krzemiński Department of Organic Chemistry, Faculty of Chemistry, Nicolaus Copernicus University in Toruń Poland [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.1.10. Preparation of (1R,2R,3R,5S)-(−)-Isopinocampheol Through a Hydroboration–Oxidation Reaction in another window
5.1.5. Synthesis of 2-Nitro-4-methylaniline p462-464 By Dulce Simão ; Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana C. Cerdeira Ana C. Cerdeira Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.1.5. Synthesis of 2-Nitro-4-methylaniline in another window
4.2.4.2. Conjugate Addition of Organocuprates to α,β-Unsaturated Ketones: Synthesis of 3,3-Dimethylcyclohexanone from 3-Methyl-2-cyclohexen-1-one p424-427 By Carlos Gregorio ; Carlos Gregorio Departamento de Química Orgánica, Facultad de Química, Universidad de Santiago de Compostela Avda. Ciencias S/N 15782 Santiago de Compostela Spain [email protected] Search for other works by this author on: This Site PubMed Google Scholar F. Javier Sardina ; F. Javier Sardina Departamento de Química Orgánica, Facultad de Química, Universidad de Santiago de Compostela Avda. Ciencias S/N 15782 Santiago de Compostela Spain [email protected] Search for other works by this author on: This Site PubMed Google Scholar Antonio Mouriño Antonio Mouriño Departamento de Química Orgánica, Facultad de Química, Universidad de Santiago de Compostela Avda. Ciencias S/N 15782 Santiago de Compostela Spain [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.4.2. Conjugate Addition of Organocuprates to α,β-Unsaturated Ketones: Synthesis of 3,3-Dimethylcyclohexanone from 3-Methyl-2-cyclohexen-1-one in another window
4.1.2.1. Synthesis of Fructone p257-260 By Thomas A. Logothetis Thomas A. Logothetis University of Southampton, Chemistry Highfield, Southampton Hampshire SO17 1BJ UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.2.1. Synthesis of Fructone in another window
5.1.6. Synthesis of 1-Nitronaphthalene p465-467 By Adam Dzielendziak Adam Dzielendziak Department of Organic Chemistry, Faculty of Chemistry, Nicolaus Copernicus University in Torun 87-100 Torun Poland [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.1.6. Synthesis of 1-Nitronaphthalene in another window
5.1.4. Regioselectivity in the Nitration of Acylanilines by Electrophilic Aromatic Substitution p456-461 By João P. Telo ; João P. Telo CQE, Department of Chemical Engineering, IST, University of Lisbon Av. Rovisco Pais 1649-003 Lisbon Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Pedro P. Santos ; Pedro P. Santos CQE, Department of Chemical Engineering, IST, University of Lisbon Av. Rovisco Pais 1649-003 Lisbon Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar João V. Moreira ; João V. Moreira CQE, Department of Chemical Engineering, IST, University of Lisbon Av. Rovisco Pais 1649-003 Lisbon Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Mariana L. Santos ; Mariana L. Santos CQE, Department of Chemical Engineering, IST, University of Lisbon Av. Rovisco Pais 1649-003 Lisbon Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana T. Batista Ana T. Batista CQE, Department of Chemical Engineering, IST, University of Lisbon Av. Rovisco Pais 1649-003 Lisbon Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.1.4. Regioselectivity in the Nitration of Acylanilines by Electrophilic Aromatic Substitution in another window
5.1.3. Synthesis of 2-(2,4-Dinitrobenzyl)pyridine p454-455 By Dulce Simão Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.1.3. Synthesis of 2-(2,4-Dinitrobenzyl)pyridine in another window
5.1.2. Halogenation Reactions of Vanillin p451-453 By Iain A. Smellie ; Iain A. Smellie School of Chemistry, University of St Andrews North Haugh, St Andrews Fife KY16 9ST UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Nigel P. Botting ; Nigel P. Botting School of Chemistry, University of St Andrews North Haugh, St Andrews Fife KY16 9ST UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Brian A. Chalmers ; Brian A. Chalmers School of Chemistry, University of St Andrews North Haugh, St Andrews Fife KY16 9ST UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Iain L. J. Patterson Iain L. J. Patterson School of Chemistry, University of St Andrews North Haugh, St Andrews Fife KY16 9ST UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.1.2. Halogenation Reactions of Vanillin in another window
5.2.2. Synthesis of 4,4′-Di- tert -butylbiphenyl p480-481 By Dulce Simão Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.2. Synthesis of 4,4′-Di-tert-butylbiphenyl in another window
5.2.4. Synthesis of 5,10,15,20-Tetrakis(2,6-dichlorophenyl)porphyrin p485-489 By Artur M. S. Silva ; Artur M. S. Silva Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Augusto C. Tomé ; Augusto C. Tomé Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Diana C. G. A. Pinto ; Diana C. G. A. Pinto Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernando M. J. Domingues ; Fernando M. J. Domingues Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Graça M. S. R. O. Rocha ; Graça M. S. R. O. Rocha Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar José A. S. Cavaleiro ; José A. S. Cavaleiro Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria da Graça ; Maria da Graça Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar P. M. S. Neves ; P. M. S. Neves Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria do Amparo F. Faustino ; Maria do Amparo F. Faustino Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Mário M. Q. Simões Mário M. Q. Simões Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.4. Synthesis of 5,10,15,20-Tetrakis(2,6-dichlorophenyl)porphyrin in another window
5.2.7. Synthesis of Musk Ketone p496-499 By João Paulo Telo João Paulo Telo CQE, Department of Chemical Engineering, IST, University of Lisbon Av. Rovisco Pais 1649-003 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.7. Synthesis of Musk Ketone in another window
5.2.6. Synthesis of 3-Bromo-7-ethylcarbamate-4-methylcoumarin p493-495 By Paula S. Branco ; Paula S. Branco Departamento de Química, Faculdade de Ciências e Tecnologia, UNL 2829-516 Caparica Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana Maria Lourenço Ana Maria Lourenço Departamento de Química, Faculdade de Ciências e Tecnologia, UNL 2829-516 Caparica Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.6. Synthesis of 3-Bromo-7-ethylcarbamate-4-methylcoumarin in another window
5.2.1. Synthesis of 1,4-Di- t -butyl-2,5-dimethoxybenzene p477-479 By Dulce Simão ; Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana C. Cerdeira Ana C. Cerdeira Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.1. Synthesis of 1,4-Di-t-butyl-2,5-dimethoxybenzene in another window
4.2.5.5. A Multicomponent Reaction of Isocyanides for the Synthesis of 4-Chromanone-2-carboxamides p443-447 By Ana G. Neo ; Ana G. Neo Departamento de Química Orgánica e Inorgánica, F. Veterinaria, Universidad de Extremadura 10071 Cáceres Spain [email protected] Search for other works by this author on: This Site PubMed Google Scholar Jesús Díaz ; Jesús Díaz Departamento de Química Orgánica e Inorgánica, F. Veterinaria, Universidad de Extremadura 10071 Cáceres Spain [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos F. Marcos Carlos F. Marcos Departamento de Química Orgánica e Inorgánica, F. Veterinaria, Universidad de Extremadura 10071 Cáceres Spain [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.5.5. A Multicomponent Reaction of Isocyanides for the Synthesis of 4-Chromanone-2-carboxamides in another window
5.2.3. Synthesis of a Macrocycle: C -Methyl[4]resorcinarene p482-484 By Christopher Baker ; Christopher Baker School of Pharmacy and Biomolecular Sciences, University of Brighton Huxley Building Brighton BN2 4GJ UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Alexander S. Cragg ; Alexander S. Cragg School of Pharmacy and Biomolecular Sciences, University of Brighton Huxley Building Brighton BN2 4GJ UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Raghuram R. Kothur ; Raghuram R. Kothur School of Pharmacy and Biomolecular Sciences, University of Brighton Huxley Building Brighton BN2 4GJ UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Flavia Fucassi ; Flavia Fucassi School of Pharmacy and Biomolecular Sciences, University of Brighton Huxley Building Brighton BN2 4GJ UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Peter J. Cragg Peter J. Cragg School of Pharmacy and Biomolecular Sciences, University of Brighton Huxley Building Brighton BN2 4GJ UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.3. Synthesis of a Macrocycle: C-Methyl[4]resorcinarene in another window
5.2.9. Synthesis of Eosin p504-507 By Dulce Simão Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.9. Synthesis of Eosin in another window
4.2.5.4. Preparation of Phenylglycine and Hydroxymorpholine Derivatives Through a Petasis Borono–Mannich Reaction p439-442 By Nuno R. Candeias ; Nuno R. Candeias Department of Chemistry and Bioengineering, Tampere University of Technology Korkeakoulunkatu 8 Tampere FI-33101 Finland [email protected] Search for other works by this author on: This Site PubMed Google Scholar Roberta Paterna ; Roberta Paterna Research Institute for Medicines and Pharmaceutical Sciences (iMed.UL), Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Pedro M. S. D. Cal ; Pedro M. S. D. Cal Research Institute for Medicines and Pharmaceutical Sciences (iMed.UL), Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Pedro M. P. Gois Pedro M. P. Gois Research Institute for Medicines and Pharmaceutical Sciences (iMed.UL), Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.5.4. Preparation of Phenylglycine and Hydroxymorpholine Derivatives Through a Petasis Borono–Mannich Reaction in another window
4.2.5.3. A Ugi Multicomponent Reaction in the Synthesis of N -Cyclohexyl-2-[ N -(4-methoxybenzyl)acetamide]-2-(thien-2-yl)acetamide p435-438 By Susana P. G. Costa ; Susana P. G. Costa University of Minho, Department of Chemistry, Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Manuela M. Raposo ; M. Manuela M. Raposo University of Minho, Department of Chemistry, Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Cátia I. C. Esteves Cátia I. C. Esteves University of Minho, Department of Chemistry, Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.5.3. A Ugi Multicomponent Reaction in the Synthesis of N-Cyclohexyl-2-[N-(4-methoxybenzyl)acetamide]-2-(thien-2-yl)acetamide in another window
4.1.2.2. Synthesis of Flavone p261-263 By Dulce Simão ; Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana C. Cerdeira Ana C. Cerdeira Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.2.2. Synthesis of Flavone in another window
5.2.10. Synthesis and Formylation of 5-Piperidino-2,2′-bithiophene p508-513 By M. Manuela M. Raposo M. Manuela M. Raposo Department of Chemistry, University of Minho, Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.10. Synthesis and Formylation of 5-Piperidino-2,2′-bithiophene in another window
6.2. Synthesis of the Antitumoral Drug 2,4,6-Tris(dimethylamino)-1,3,5-triazine via Sequential Nucleophilic Substitution p535-538 By Filipa Siopa ; Filipa Siopa Instituto de Investigação, do Medicamento (iMed.ULisboa), Faculdade de Farmácia, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Nuno Candeias ; Nuno Candeias Department of Chemistry and Bioengineering, Tampere University of Technology Korkeakoulunkatu 8 Tampere FI-33101 Finland [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso Instituto de Investigação, do Medicamento (iMed.ULisboa), Faculdade de Farmácia, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 6.2. Synthesis of the Antitumoral Drug 2,4,6-Tris(dimethylamino)-1,3,5-triazine via Sequential Nucleophilic Substitution in another window
5.2.5. Solventless Synthesis, Separation and Characterization of Zinc and Free-Base Tetraphenyl Porphyrin p490-492 By Waqar Rizvi ; Waqar Rizvi Hunter College of the City University of New York 695 Park Avenue New York New York 10065 USA The Graduate Center of the City University of New York 365 Fifth Avenue New York New York 10016 USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar Charles M. Drain ; Charles M. Drain Hunter College of the City University of New York 695 Park Avenue New York New York 10065 USA The Graduate Center of the City University of New York 365 Fifth Avenue New York New York 10016 USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar Patrick Moy ; Patrick Moy Hunter College of the City University of New York 695 Park Avenue New York New York 10065 USA Search for other works by this author on: This Site PubMed Google Scholar Matthew J. Jurow Matthew J. Jurow The Molecular Foundry, Lawrence Berkeley National Laboratory Berkeley California 94720 USA Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.5. Solventless Synthesis, Separation and Characterization of Zinc and Free-Base Tetraphenyl Porphyrin in another window
5.1.8. Preparation of p -Bromoaniline p472-476 By Abel J. S. C. Vieira Abel J. S. C. Vieira Faculty of Sciences and Technology, Universidade Nova de Lisboa 2829-516 Caparica Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.1.8. Preparation of p-Bromoaniline in another window
6.3. Benzotriazole, a Useful Synthetic Auxiliary in Heterocyclizations p539-541 By João Lavrado ; João Lavrado Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Marta Figueiras ; Marta Figueiras Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Eduardo Ruivo ; Eduardo Ruivo Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Susana Lucas ; Susana Lucas Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Alexandra Paulo Alexandra Paulo Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] Pharmaceutical and Medicinal Chemistry Department, Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 6.3. Benzotriazole, a Useful Synthetic Auxiliary in Heterocyclizations in another window
5.1.7. Selective Boc-Protection and Bromination of Pyrazoles p468-471 By Thomas A. Logothetis Thomas A. Logothetis University of Southampton, Chemistry, Highfield Southampton Hampshire SO17 1BJ UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.1.7. Selective Boc-Protection and Bromination of Pyrazoles in another window
4.1.2.3. Synthesis and Characterisation of H 2 salen: An Introduction to 1D and 2D NMR Spectroscopy p264-268 By Maria J. Villa de Brito Maria J. Villa de Brito DQB, CQE, Faculdade de Ciências da Universidade de Lisboa Campo Grande, 1749-001 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.2.3. Synthesis and Characterisation of H2salen: An Introduction to 1D and 2D NMR Spectroscopy in another window
4.1.2.4. Synthesis of Lophine and Conversion into Dimers p269-271 By Dulce Simão Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.2.4. Synthesis of Lophine and Conversion into Dimers in another window
6.4. Synthesis of 4,5-Dicyanobenzene-1,2-dithiol p542-544 By Dulce Simão Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 6.4. Synthesis of 4,5-Dicyanobenzene-1,2-dithiol in another window
4.1.2.5. Synthesis of Dibenzalacetone 2,4-Dinitrophenylhydrazone p272-276 By Ana Margarida Madureira ; Ana Margarida Madureira Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana Bela Santana ; Ana Bela Santana Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Emília Valente ; Emília Valente Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria-José U. Ferreira Maria-José U. Ferreira Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.2.5. Synthesis of Dibenzalacetone 2,4-Dinitrophenylhydrazone in another window
4.1.2.6. Synthesis and Structural Characterization of an Antitubercular Isoniazid Hydrazone p277-281 By Susana Santos ; Susana Santos Centro de Química e Bioquímica, Departamento de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa Ed. C8 Campo Grande, 1749-016 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Filomena Martins Filomena Martins Centro de Química e Bioquímica, Departamento de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa Ed. C8 Campo Grande, 1749-016 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.2.6. Synthesis and Structural Characterization of an Antitubercular Isoniazid Hydrazone in another window
7.3. Recycling Bromovanillin into Ferulic Acid-Based Antioxidants p559-563 By Tiago Silva ; Tiago Silva CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences, University of Porto Rua do Campo Alegre s/n 4169-007 Porto Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Daniel Chavarria ; Daniel Chavarria CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences, University of Porto Rua do Campo Alegre s/n 4169-007 Porto Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Lisa Sequeira ; Lisa Sequeira CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences, University of Porto Rua do Campo Alegre s/n 4169-007 Porto Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernanda Borges Fernanda Borges CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences, University of Porto Rua do Campo Alegre s/n 4169-007 Porto Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 7.3. Recycling Bromovanillin into Ferulic Acid-Based Antioxidants in another window
4.1.2.7. Preparation of a Tosylhydrazidyl N -Glycosyl Derivative of d -Glucuronic Acid via Tosylhydrazone Formation and Intramolecular Ring Closure p282-284 By Nuno M. Xavier Nuno M. Xavier Centro de Química e Bioquímica, Faculdade de Ciências, Universidade de Lisboa 1749-016 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.2.7. Preparation of a Tosylhydrazidyl N-Glycosyl Derivative of d-Glucuronic Acid via Tosylhydrazone Formation and Intramolecular Ring Closure in another window
7.4. Sonogashira Coupling Reaction of Aryl Derivatives: A Versatile Method for Acetylide Building Blocks p564-567 By Tiago J. Silva ; Tiago J. Silva Centro de Ciências Moleculares de Materiais, Faculdade de Ciências da Universidade de Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Paulo J. Mendes ; Paulo J. Mendes Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora Évora Portugal Search for other works by this author on: This Site PubMed Google Scholar António P. S. Teixeira ; António P. S. Teixeira Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora Évora Portugal Search for other works by this author on: This Site PubMed Google Scholar M. Paula Robalo ; M. Paula Robalo Área Departamental de Engenharia Química, Instituto Superior de Engenharia de Lisboa Portugal Centro de Química Estrutural, Complexo I, Instituto Superior Técnico, Universidade de Lisboa Portugal Search for other works by this author on: This Site PubMed Google Scholar M. H. Garcia M. H. Garcia Centro de Ciências Moleculares de Materiais, Faculdade de Ciências da Universidade de Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 7.4. Sonogashira Coupling Reaction of Aryl Derivatives: A Versatile Method for Acetylide Building Blocks in another window
5.2.11. Synthesis of 3-Bromosalicylaldehyde by Ortho -formylation of 2-Bromophenol p514-516 By Trond Vidar Hansen ; Trond Vidar Hansen Department of Pharmaceutical Chemistry, School of Pharmacy, University of Oslo PO Box 1068 Blindern N-0316 Oslo Norway [email protected] Search for other works by this author on: This Site PubMed Google Scholar Lars Skattebøl Lars Skattebøl Department of Chemistry, University of Oslo PO Box 1033 Blindern N-0315 Oslo Norway Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.11. Synthesis of 3-Bromosalicylaldehyde by Ortho-formylation of 2-Bromophenol in another window
6.1. Synthesis of 2,3-Quinoxalinedithiol p532-534 By Dulce Simão ; Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana C. Cerdeira Ana C. Cerdeira Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 6.1. Synthesis of 2,3-Quinoxalinedithiol in another window
5.2.12. Synthesis of Indolo[3,2- b ]quinolin-11-one by Acid-Catalysed Intramolecular Double Cyclization p517-521 By João Lavrado ; João Lavrado Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649 003 Lisboa Portugal Search for other works by this author on: This Site PubMed Google Scholar Marta Figueiras ; Marta Figueiras Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649 003 Lisboa Portugal Search for other works by this author on: This Site PubMed Google Scholar David M. Pereira ; David M. Pereira Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649 003 Lisboa Portugal Search for other works by this author on: This Site PubMed Google Scholar Sofia A. Santos ; Sofia A. Santos Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649 003 Lisboa Portugal Search for other works by this author on: This Site PubMed Google Scholar Rui Moreira ; Rui Moreira Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649 003 Lisboa Portugal Pharmaceutical and Medicinal Chemistry Department, Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649 003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Alexandra Paulo Alexandra Paulo Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649 003 Lisboa Portugal Pharmaceutical and Medicinal Chemistry Department, Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649 003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.12. Synthesis of Indolo[3,2-b]quinolin-11-one by Acid-Catalysed Intramolecular Double Cyclization in another window
4.1.3.1. Green Metrics in a Cyclocondensation Reaction p285-289 By Clarissa P. Frizzo ; Clarissa P. Frizzo Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Marcos A. P. Martins ; Marcos A. P. Martins Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Paulo R. S. Salbego ; Paulo R. S. Salbego Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Caroline R. Bender ; Caroline R. Bender Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Aniele Z. Tier ; Aniele Z. Tier Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Hélio G. Bonacorso Hélio G. Bonacorso Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.3.1. Green Metrics in a Cyclocondensation Reaction in another window
4.1.3.2. Synthesis of 1 H -Pyrazoles Using Ball Mill, Grinding and Conventional Thermal Heating p290-293 By Clarissa P. Frizzo ; Clarissa P. Frizzo Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Marcos A. P. Martins ; Marcos A. P. Martins Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Caroline R. Bender ; Caroline R. Bender Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Paulo R. S. Salbego ; Paulo R. S. Salbego Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Aniele Z. Tier ; Aniele Z. Tier Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Guilherme C. Paveglio ; Guilherme C. Paveglio Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Kelvis Longhi Kelvis Longhi Núcleo de Química de Heterociclos (NUQUIMHE), Department of Chemistry, Federal University of Santa Maria 97105-900 Santa Maria RS Brazil [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.3.2. Synthesis of 1H-Pyrazoles Using Ball Mill, Grinding and Conventional Thermal Heating in another window
5.2.8. Synthesis of Methyl 4-oxo-4-(thiophen-2-yl)butanoate p500-503 By M. Manuela M. Raposo M. Manuela M. Raposo Department of Chemistry, University of Minho, Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.8. Synthesis of Methyl 4-oxo-4-(thiophen-2-yl)butanoate in another window
5.2.13. Mild and Fast Friedel–Crafts Acylation Over Zeolites p522-525 By A. F. Brigas ; A. F. Brigas Universidade do Algarve, Departamento de Química e Farmácia, Centro de Investigação em Química do Algarve (CIQA), Campus de Gambelas 8005-139 Faro Portugal Universidade de Lisboa, Faculdade de Ciências, Centro de Química e Bioquímica (CQB) C8, Campo Grande 1749-016 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar F. Martins ; F. Martins Universidade de Lisboa, Faculdade de Ciências, Centro de Química e Bioquímica (CQB) C8, Campo Grande 1749-016 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar R. Elvas-Leitão ; R. Elvas-Leitão Universidade de Lisboa, Faculdade de Ciências, Centro de Química e Bioquímica (CQB) C8, Campo Grande 1749-016 Lisboa Portugal [email protected] Instituto Politécnico de Lisboa, Instituto Superior de Engenharia de Lisboa (ISEL), Área Departamental de Engenharia Química Rua Conselheiro Emídio Navarro, 1 1959-007 Lisboa Portugal Search for other works by this author on: This Site PubMed Google Scholar B. S. Santos ; B. S. Santos Universidade de Coimbra, Departamento de Química 3004-535 Coimbra Portugal Search for other works by this author on: This Site PubMed Google Scholar A. Martins ; A. Martins Universidade de Lisboa, Faculdade de Ciências, Centro de Química e Bioquímica (CQB) C8, Campo Grande 1749-016 Lisboa Portugal [email protected] Instituto Politécnico de Lisboa, Instituto Superior de Engenharia de Lisboa (ISEL), Área Departamental de Engenharia Química Rua Conselheiro Emídio Navarro, 1 1959-007 Lisboa Portugal Search for other works by this author on: This Site PubMed Google Scholar N. Nunes N. Nunes Universidade de Lisboa, Faculdade de Ciências, Centro de Química e Bioquímica (CQB) C8, Campo Grande 1749-016 Lisboa Portugal [email protected] Instituto Politécnico de Lisboa, Instituto Superior de Engenharia de Lisboa (ISEL), Área Departamental de Engenharia Química Rua Conselheiro Emídio Navarro, 1 1959-007 Lisboa Portugal Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.13. Mild and Fast Friedel–Crafts Acylation Over Zeolites in another window
4.1.3.3. Organocatalytic Enantioselective Michael Addition of Thiophenol to Chalcone p294-297 By Mariola Zielińska-Błajet ; Mariola Zielińska-Błajet Department of Organic Chemistry, Faculty of Chemistry, Wrocław University of Technology Wyb. Wyspiańskiego 27 50-370 Wrocław Poland [email protected] Search for other works by this author on: This Site PubMed Google Scholar Jacek Skarżewski Jacek Skarżewski Department of Organic Chemistry, Faculty of Chemistry, Wrocław University of Technology Wyb. Wyspiańskiego 27 50-370 Wrocław Poland [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.3.3. Organocatalytic Enantioselective Michael Addition of Thiophenol to Chalcone in another window
7.9. An Efficient Methodology for the Synthesis of the 3-Styryl Coumarin p584-587 By António Manuel D. R. L. Pereira ; António Manuel D. R. L. Pereira Departamento de Química, Escola de Ciências e Tecnologia, Universidade de Évora, Colégio Luís António Verney Rua Romão Ramalho, N° 59 7000-671 Portugal Laboratório HERCULES, Universidade de Évora Largo Marquês de Marialva, N° 8 7000-809 Évora Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Sérgio Miguel A. Martins Sérgio Miguel A. Martins Laboratório HERCULES, Universidade de Évora Largo Marquês de Marialva, N° 8 7000-809 Évora Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 7.9. An Efficient Methodology for the Synthesis of the 3-Styryl Coumarin in another window
7.5. Convergent Synthesis of a Suzuki Product p568-572 By Thomas A. Logothetis Thomas A. Logothetis University of Southampton, Chemistry, Highfield Southampton Hampshire SO17 1BJ UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 7.5. Convergent Synthesis of a Suzuki Product in another window
7.10. Sonogashira Coupling Between a Vinylic Halide and a Terminal Alkyne p588-591 By Carine Maaliki ; Carine Maaliki UFR Sciences et Techniques de Tours, Parc Grandmont, Bat Yves Chauvin 32 Av. Monge 37200 Tours France [email protected] Search for other works by this author on: This Site PubMed Google Scholar Jérôme Thibonnet Jérôme Thibonnet UFR Sciences et Techniques de Tours, Parc Grandmont, Bat Yves Chauvin 32 Av. Monge 37200 Tours France [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 7.10. Sonogashira Coupling Between a Vinylic Halide and a Terminal Alkyne in another window
5.2.14. Reactivity Studies of 1-Propyl-2-(thiophen-2-yl)-1 H -pyrrole p526-531 By Maria Manuela Marques Raposo ; Maria Manuela Marques Raposo University of Minho, Department of Chemistry, Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Sara Sofia Marques Fernandes ; Sara Sofia Marques Fernandes University of Minho, Department of Chemistry, Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria Cidália Rodrigues Castro Maria Cidália Rodrigues Castro University of Minho, Department of Chemistry, Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 5.2.14. Reactivity Studies of 1-Propyl-2-(thiophen-2-yl)-1H-pyrrole in another window
7.6. Oxidative Heck Reaction at Room Temperature p573-576 By Rajiv T. Sawant ; Rajiv T. Sawant Organic Pharmaceutical Chemistry, Department of Medicinal Chemistry, Uppsala University Biomedical Center Box 574, SE-751 23 Uppsala Sweden [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ashkan Fardost ; Ashkan Fardost Organic Pharmaceutical Chemistry, Department of Medicinal Chemistry, Uppsala University Biomedical Center Box 574, SE-751 23 Uppsala Sweden [email protected] Search for other works by this author on: This Site PubMed Google Scholar Luke R. Odell Luke R. Odell Organic Pharmaceutical Chemistry, Department of Medicinal Chemistry, Uppsala University Biomedical Center Box 574, SE-751 23 Uppsala Sweden [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 7.6. Oxidative Heck Reaction at Room Temperature in another window
4.1.3.4. Stereoselective Synthesis of meso -1-Allyl-2,6-diphenylpiperidin-4-one p298-300 By Ana-Belén García Delgado ; Ana-Belén García Delgado Departamento de Química Orgánica e Inorgánica, Facultad de Químicas, Universidad de Oviedo Spain [email protected] Search for other works by this author on: This Site PubMed Google Scholar Noelia Quiñones ; Noelia Quiñones Departamento de Química Orgánica e Inorgánica, Facultad de Químicas, Universidad de Oviedo Spain [email protected] Search for other works by this author on: This Site PubMed Google Scholar María-Paz Cabal María-Paz Cabal Departamento de Química Orgánica e Inorgánica, Facultad de Químicas, Universidad de Oviedo Spain [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.3.4. Stereoselective Synthesis of meso-1-Allyl-2,6-diphenylpiperidin-4-one in another window
4.1.3.5. Synthesis of a Squarylium Cyanine Dye as Potential Photosensitizer for Photodynamic Therapy (PDT) p301-305 By Marlene L. F. M. Pacheco ; Marlene L. F. M. Pacheco Department of Chemistry and CQ-VR, UTAD Quinta de Prados 5000-801 Vila Real Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Sofia F. P. Friães ; Sofia F. P. Friães Department of Chemistry and CQ-VR, UTAD Quinta de Prados 5000-801 Vila Real Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Renato E. Boto ; Renato E. Boto CICS-UBI – Health Sciences Research Centre, University of Beira Interior Av. Infante D. Henrique 6200-506 Covilhã Portugal Search for other works by this author on: This Site PubMed Google Scholar Paulo Almeida ; Paulo Almeida CICS-UBI – Health Sciences Research Centre, University of Beira Interior Av. Infante D. Henrique 6200-506 Covilhã Portugal Search for other works by this author on: This Site PubMed Google Scholar Amélia M. Silva ; Amélia M. Silva Department of Biology and Environment and CITAB, UTAD Quinta de Prados 5000-801 Vila Real Portugal Search for other works by this author on: This Site PubMed Google Scholar Lucinda V. Reis Lucinda V. Reis Department of Chemistry and CQ-VR, UTAD Quinta de Prados 5000-801 Vila Real Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.1.3.5. Synthesis of a Squarylium Cyanine Dye as Potential Photosensitizer for Photodynamic Therapy (PDT) in another window
4.2.1.1. The Effects of Stoichiometry and Starting Material on the Product Identity and Yield in Grignard Addition Reactions p306-311 By Jane Brock Greco ; Jane Brock Greco Department of Chemistry, Johns Hopkins University 3400 N. Charles St. Baltimore MD 21218 USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar Eric Hill Eric Hill Department of Chemistry, Johns Hopkins University 3400 N. Charles St. Baltimore MD 21218 USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.1.1. The Effects of Stoichiometry and Starting Material on the Product Identity and Yield in Grignard Addition Reactions in another window
7.7. Synthesis of 2-Methyl-1,1′-binaphthalene via Suzuki Cross-Coupling Reaction p577-580 By Javier Iglesias-Sigüenza ; Javier Iglesias-Sigüenza Departamento de Química Orgánica, Universidad de Sevilla C/ Profesor García González, n°1 41012-Sevilla Spain [email protected] Search for other works by this author on: This Site PubMed Google Scholar David Monge ; David Monge Departamento de Química Orgánica, Universidad de Sevilla C/ Profesor García González, n°1 41012-Sevilla Spain [email protected] Search for other works by this author on: This Site PubMed Google Scholar Elena Díez Elena Díez Departamento de Química Orgánica, Universidad de Sevilla C/ Profesor García González, n°1 41012-Sevilla Spain [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 7.7. Synthesis of 2-Methyl-1,1′-binaphthalene via Suzuki Cross-Coupling Reaction in another window
7.8. Green Synthesis of Aromatic Ketones: Decarboxylative Palladium Catalysis Under Microwave Irradiation p581-583 By Jonas Sävmarker ; Jonas Sävmarker Organic Pharmaceutical Chemistry, Department of Medicinal Chemistry, Uppsala University Biomedical Center Box 574, SE-751 23 Uppsala Sweden [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ashkan Fardost ; Ashkan Fardost Organic Pharmaceutical Chemistry, Department of Medicinal Chemistry, Uppsala University Biomedical Center Box 574, SE-751 23 Uppsala Sweden [email protected] Search for other works by this author on: This Site PubMed Google Scholar Luke R. Odell Luke R. Odell Organic Pharmaceutical Chemistry, Department of Medicinal Chemistry, Uppsala University Biomedical Center Box 574, SE-751 23 Uppsala Sweden [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 7.8. Green Synthesis of Aromatic Ketones: Decarboxylative Palladium Catalysis Under Microwave Irradiation in another window
6.5. Nucleophilic Aromatic Substitution Reactions in 3,6-Bis(3,5-dimethyl-1 H -pyrazol-1-yl)-1,2,4,5-tetrazine p545-549 By Tiago J. L. Silva ; Tiago J. L. Silva Centro de Química Estrutural, Faculdade de Ciências da Universidade de Lisboa Campo Grande 1049-016 Campo Grande, Lisboa Portugal Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora Rua Romão Ramalho 59 7000-671 Évora Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Paulo J. G. Mendes ; Paulo J. G. Mendes Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora Rua Romão Ramalho 59 7000-671 Évora Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana Isabel Tomaz ; Ana Isabel Tomaz Centro de Química Estrutural, Faculdade de Ciências da Universidade de Lisboa Campo Grande 1049-016 Campo Grande, Lisboa Portugal Search for other works by this author on: This Site PubMed Google Scholar M. Helena Garcia M. Helena Garcia Centro de Química Estrutural, Faculdade de Ciências da Universidade de Lisboa Campo Grande 1049-016 Campo Grande, Lisboa Portugal Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 6.5. Nucleophilic Aromatic Substitution Reactions in 3,6-Bis(3,5-dimethyl-1H-pyrazol-1-yl)-1,2,4,5-tetrazine in another window
4.2.1.2. Synthesis of Methyl Triphenylmethyl Ether p312-315 By Dulce Simão ; Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana C. Cerdeira Ana C. Cerdeira Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.1.2. Synthesis of Methyl Triphenylmethyl Ether in another window
4.2.1.3. Grignard-Like Reaction in Water p316-318 By João R. Vale ; João R. Vale iMed.UL, Faculdade de Farmácia da Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso iMed.UL, Faculdade de Farmácia da Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.1.3. Grignard-Like Reaction in Water in another window
7.1. A Solvent-Free Ullmann Coupling: Synthesis of 2,2′-Dinitrobiphenyl p550-553 By Laurel Goj Habgood ; Laurel Goj Habgood Rollins College 1000 Holt Avenue, Box 2743 Winter Park FL 32789 USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar Richard W. Gregor Richard W. Gregor Rollins College 1000 Holt Avenue, Box 2743 Winter Park FL 32789 USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 7.1. A Solvent-Free Ullmann Coupling: Synthesis of 2,2′-Dinitrobiphenyl in another window
4.2.1.4. Cram’s Rule – Diastereoselective Grignard Addition to 2-Phenylpropanal p319-321 By Laura M. Hancock ; Laura M. Hancock Lennard-Jones Laboratories, School of Physical and Geographical Sciences, Keele University Staffordshire ST5 5BG UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Michael G. Edwards ; Michael G. Edwards Lennard-Jones Laboratories, School of Physical and Geographical Sciences, Keele University Staffordshire ST5 5BG UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Graeme R. Jones ; Graeme R. Jones Lennard-Jones Laboratories, School of Physical and Geographical Sciences, Keele University Staffordshire ST5 5BG UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Matthew O’Brien Matthew O’Brien Lennard-Jones Laboratories, School of Physical and Geographical Sciences, Keele University Staffordshire ST5 5BG UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.1.4. Cram’s Rule – Diastereoselective Grignard Addition to 2-Phenylpropanal in another window
7.2. Reactivity Studies for the Synthesis of 5-Phenylthiophene-2-carbaldehyde by a Suzuki–Miyaura Coupling p554-558 By Maria Manuela Marques Raposo ; Maria Manuela Marques Raposo University of Minho, Department of Chemistry, Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Susana Paula Graça da Costa ; Susana Paula Graça da Costa University of Minho, Department of Chemistry, Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Rosa Maria Ferreira Batista ; Rosa Maria Ferreira Batista University of Minho, Department of Chemistry, Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Rosa Cristina Moutinho Ferreira Rosa Cristina Moutinho Ferreira University of Minho, Department of Chemistry, Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 7.2. Reactivity Studies for the Synthesis of 5-Phenylthiophene-2-carbaldehyde by a Suzuki–Miyaura Coupling in another window
4.2.1.5. Preparation of (4 R ,5 R )-4,5-Bis(diphenylhydroxymethyl)-2,2-dimethyldioxolane ((−)-TADDOL) p322-326 By Naylil M. R. Capreti ; Naylil M. R. Capreti Institute of Chemistry, State University of Campinas C.P. 6154 13083-970 Campinas SP Brazil [email protected] Search for other works by this author on: This Site PubMed Google Scholar Igor D. Jurberg Igor D. Jurberg Institute of Chemistry, State University of Campinas C.P. 6154 13083-970 Campinas SP Brazil [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.1.5. Preparation of (4R,5R)-4,5-Bis(diphenylhydroxymethyl)-2,2-dimethyldioxolane ((−)-TADDOL) in another window
4.2.1.6. Synthesis of ( S )-Diphenyl(pyrrolidin-2-yl)methanol p327-330 By David Monge ; David Monge Departamento de Química Orgánica, Universidad de Sevilla C/ Prof. García González, no. 1 41012-Sevilla Spain [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Javier Iglesias-Sigüenza ; Javier Iglesias-Sigüenza Departamento de Química Orgánica, Universidad de Sevilla C/ Prof. García González, no. 1 41012-Sevilla Spain [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Elena Díez Elena Díez Departamento de Química Orgánica, Universidad de Sevilla C/ Prof. García González, no. 1 41012-Sevilla Spain [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.1.6. Synthesis of (S)-Diphenyl(pyrrolidin-2-yl)methanol in another window
4.2.2.1. Solvent-Free Aldol Condensation Reactions: Synthesis of Chalcone Derivatives p331-334 By Barbora Morra ; Barbora Morra Department of Chemistry, University of Toronto Toronto Ontario Canada M5S 3H6 [email protected] Search for other works by this author on: This Site PubMed Google Scholar Connie Tang ; Connie Tang Department of Chemistry, University of Toronto Toronto Ontario Canada M5S 3H6 [email protected] Search for other works by this author on: This Site PubMed Google Scholar Jonathon Fossella Jonathon Fossella Department of Chemistry, University of Toronto Toronto Ontario Canada M5S 3H6 [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.2.1. Solvent-Free Aldol Condensation Reactions: Synthesis of Chalcone Derivatives in another window
4.2.2.2. Synthesis of ( E )-Chalcones [( E )-1,3-diarylprop-2-en-1-ones] p335-338 By Artur M. S. Silva ; Artur M. S. Silva Chemistry Department & QOPNA, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Augusto C. Tomé ; Augusto C. Tomé Chemistry Department & QOPNA, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Diana C. G. A. Pinto ; Diana C. G. A. Pinto Chemistry Department & QOPNA, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernando Domingues ; Fernando Domingues Chemistry Department & QOPNA, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Graça M. Oliveira Rocha ; Graça M. Oliveira Rocha Chemistry Department & QOPNA, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar José A. S. Cavaleiro ; José A. S. Cavaleiro Chemistry Department & QOPNA, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Graça P. M. S. Neves ; M. Graça P. M. S. Neves Chemistry Department & QOPNA, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Amparo F. Faustino ; M. Amparo F. Faustino Chemistry Department & QOPNA, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Mário M. Q. Simões Mário M. Q. Simões Chemistry Department & QOPNA, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.2.2. Synthesis of (E)-Chalcones [(E)-1,3-diarylprop-2-en-1-ones] in another window
4.2.2.3. A Solvent-Free Approach for Chalcone Synthesis via an Aldol Reaction p339-341 By Sofia F. P. Friães ; Sofia F. P. Friães Department of Chemistry and CQ-VR, UTAD Quinta de Prados 5000-801 Vila Real Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Renato E. Boto ; Renato E. Boto CICS-UBI – Health Sciences Research Centre, University of Beira Interior Av. Infante D. Henrique 6200-506 Covilhã Portugal Search for other works by this author on: This Site PubMed Google Scholar Paulo Almeida ; Paulo Almeida CICS-UBI – Health Sciences Research Centre, University of Beira Interior Av. Infante D. Henrique 6200-506 Covilhã Portugal Search for other works by this author on: This Site PubMed Google Scholar Amélia M. Silva ; Amélia M. Silva Department of Biology and Environment and CITAB, UTAD Quinta de Prados 5000-801 Vila Real Portugal Search for other works by this author on: This Site PubMed Google Scholar Lucinda V. Reis Lucinda V. Reis Department of Chemistry and CQ-VR, UTAD Quinta de Prados 5000-801 Vila Real Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.2.3. A Solvent-Free Approach for Chalcone Synthesis via an Aldol Reaction in another window
4.2.2.4. Preparation of Dibenzylideneacetone p342-344 By Abel J. S. C. Vieira Abel J. S. C. Vieira Faculty of Sciences and Technology, Universidade Nova de Lisboa 2829-516 Caparica Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.2.4. Preparation of Dibenzylideneacetone in another window
4.2.2.5. l -Proline Catalyzed Aldol Reaction of 4-Nitrobenzaldehyde with Acetone p345-347 By Fang Fang ; Fang Fang Department of Chemistry, South University of Science and Technology of China Shenzhen 518055 People’s Republic of China [email protected] Search for other works by this author on: This Site PubMed Google Scholar Xin-Yuan Liu ; Xin-Yuan Liu Department of Chemistry, South University of Science and Technology of China Shenzhen 518055 People’s Republic of China [email protected] Search for other works by this author on: This Site PubMed Google Scholar Bin Tan Bin Tan Department of Chemistry, South University of Science and Technology of China Shenzhen 518055 People’s Republic of China [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.2.5. l-Proline Catalyzed Aldol Reaction of 4-Nitrobenzaldehyde with Acetone in another window
4.2.2.6. Preparation of a β -Nitrostyrene Derivative by the Henry Reaction: Comparison of a Conventional and a Microwave-Assisted Method p348-351 By Daniel Martins ; Daniel Martins CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences of University of Porto Portugal Search for other works by this author on: This Site PubMed Google Scholar Joana Reis ; Joana Reis CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences of University of Porto Portugal Search for other works by this author on: This Site PubMed Google Scholar Fernanda Borges ; Fernanda Borges CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences of University of Porto Portugal Search for other works by this author on: This Site PubMed Google Scholar Nuno Milhazes Nuno Milhazes CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences of University of Porto Portugal CESPU/Superior Institute of Health of Sciences – North Rua Central de Gandra, 1317 4585-116 Gandra PRD Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.2.6. Preparation of a β-Nitrostyrene Derivative by the Henry Reaction: Comparison of a Conventional and a Microwave-Assisted Method in another window
4.2.2.7. Synthesis of Aurone Derivatives Through Acid-Catalysed Aldol Condensation p352-354 By Ana R. Duarte ; Ana R. Duarte Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Professor Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Marta P. Carrasco ; Marta P. Carrasco Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Professor Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana S. Ressurreição Ana S. Ressurreição Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Professor Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.2.7. Synthesis of Aurone Derivatives Through Acid-Catalysed Aldol Condensation in another window
4.2.2.8. Synthesis of Pyrazole Heterocycles p355-358 By Thomas A. Logothetis Thomas A. Logothetis University of Southampton, Chemistry, Highfield Southampton Hampshire SO17 1BJ UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.2.8. Synthesis of Pyrazole Heterocycles in another window
4.2.2.9. A Green Approach to 3-Carbonylchromones p359-362 By Ana Bornadiego ; Ana Bornadiego Departamento de Química e Inorgánica. F. Veterinaria, Universidad de Extremadura 10071 Cáceres Spain [email protected] Search for other works by this author on: This Site PubMed Google Scholar Jesús Díaz ; Jesús Díaz Departamento de Química e Inorgánica. F. Veterinaria, Universidad de Extremadura 10071 Cáceres Spain [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana G. Neo ; Ana G. Neo Departamento de Química e Inorgánica. F. Veterinaria, Universidad de Extremadura 10071 Cáceres Spain [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos F. Marcos Carlos F. Marcos Departamento de Química e Inorgánica. F. Veterinaria, Universidad de Extremadura 10071 Cáceres Spain [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.2.9. A Green Approach to 3-Carbonylchromones in another window
4.2.2.10. Synthesis of Indigo and Dyeing Process p363-365 By Dulce Simão Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.2.10. Synthesis of Indigo and Dyeing Process in another window
4.2.3.1. Knorr Pyrazole Synthesis of Edaravone p366-369 By Ana Paula Francisco ; Ana Paula Francisco Instituto de Investigação do Medicamento (iMed.ULisboa), Faculdade de Farmácia da, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana S. Ressurreição ; Ana S. Ressurreição Instituto de Investigação do Medicamento (iMed.ULisboa), Faculdade de Farmácia da, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria de Jesus Perry ; Maria de Jesus Perry Instituto de Investigação do Medicamento (iMed.ULisboa), Faculdade de Farmácia da, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Francisca Lopes Francisca Lopes Instituto de Investigação do Medicamento (iMed.ULisboa), Faculdade de Farmácia da, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.3.1. Knorr Pyrazole Synthesis of Edaravone in another window
4.2.3.2. Greener Solvent Substitution in a Verley–Doebner Condensation p370-372 By Jonathon W. Moir ; Jonathon W. Moir Department of Chemistry, University of Toronto 80 St. George Street Toronto Ontario Canada M5S 3H6 [email protected] Search for other works by this author on: This Site PubMed Google Scholar Andrew P. Dicks Andrew P. Dicks Department of Chemistry, University of Toronto 80 St. George Street Toronto Ontario Canada M5S 3H6 [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.3.2. Greener Solvent Substitution in a Verley–Doebner Condensation in another window
4.2.3.3. Knorr Synthesis of Diethyl 3,5-Dimethyl-1 H -pyrrole-2,4-dicarboxylate p373-375 By M. Soledad Pino-González ; M. Soledad Pino-González Organic Chemistry Department, Faculty of Sciences, University of Málaga 29071 Málaga Spain [email protected] Search for other works by this author on: This Site PubMed Google Scholar Cristina García-Ruiz ; Cristina García-Ruiz Organic Chemistry Department, Faculty of Sciences, University of Málaga 29071 Málaga Spain [email protected] Search for other works by this author on: This Site PubMed Google Scholar Francisco Sarabia ; Francisco Sarabia Organic Chemistry Department, Faculty of Sciences, University of Málaga 29071 Málaga Spain [email protected] Search for other works by this author on: This Site PubMed Google Scholar Gregorio Torres Gregorio Torres Organic Chemistry Department, Faculty of Sciences, University of Málaga 29071 Málaga Spain [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.3.3. Knorr Synthesis of Diethyl 3,5-Dimethyl-1H-pyrrole-2,4-dicarboxylate in another window
4.2.3.4. Synthesis of Coumarin-3-carboxylic Acid p376-379 By Paulo Coelho ; Paulo Coelho Centro de Química – Vila Real, Universidade de Trás-os-Montes e Alto Douro 5001-801 Vila Real Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Céu Sousa Céu Sousa Centro de Química – Vila Real, Universidade de Trás-os-Montes e Alto Douro 5001-801 Vila Real Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.3.4. Synthesis of Coumarin-3-carboxylic Acid in another window
4.2.3.5. Synthesis of Lipophilic Antioxidants Based on Natural Models p380-386 By Sofia Benfeito ; Sofia Benfeito CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences, University of Porto Porto Portugal Search for other works by this author on: This Site PubMed Google Scholar Tiago Silva ; Tiago Silva CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences, University of Porto Porto Portugal Search for other works by this author on: This Site PubMed Google Scholar Diogo Magalhães Silva ; Diogo Magalhães Silva CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences, University of Porto Porto Portugal Search for other works by this author on: This Site PubMed Google Scholar E. Manuela Garrido ; E. Manuela Garrido CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences, University of Porto Porto Portugal Department of Chemical Engineering, School of Engineering (ISEP), Polytechnic of Porto Porto Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernanda Borges ; Fernanda Borges CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences, University of Porto Porto Portugal Search for other works by this author on: This Site PubMed Google Scholar Jorge Garrido Jorge Garrido CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences, University of Porto Porto Portugal Department of Chemical Engineering, School of Engineering (ISEP), Polytechnic of Porto Porto Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.3.5. Synthesis of Lipophilic Antioxidants Based on Natural Models in another window
4.2.3.6. A Simple and Ecological Preparation of a Chromene-3-carboxamide Derivative p387-390 By Marta Costa ; Marta Costa Chemistry Department, University of Minho, Campus de Gualtar 4710 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Fernanda Proença M. Fernanda Proença Chemistry Department, University of Minho, Campus de Gualtar 4710 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.3.6. A Simple and Ecological Preparation of a Chromene-3-carboxamide Derivative in another window
4.2.3.7. Synthesis of a Biologically Active Oxazol-5(4 H )-One via Erlenmeyer–Plöchl Reaction p391-395 By Catarina A. B. Rodrigues ; Catarina A. B. Rodrigues Instituto de Investigação do Medicamento (iMed.ULisboa), Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar José M. G. Martinho ; José M. G. Martinho Centro de Química-Física Molecular and IN-Institute of Nanoscience and Nanothecnology, Instituto Superior Técnico Av. Rovisco Pais 1049-001 Lisboa Portugal Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso Instituto de Investigação do Medicamento (iMed.ULisboa), Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 4.2.3.7. Synthesis of a Biologically Active Oxazol-5(4H)-One via Erlenmeyer–Plöchl Reaction in another window
8.1. Synthesis of Dulcin p592-594 By Dulce Simão Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 8.1. Synthesis of Dulcin in another window
8.2. Microwave-Assisted Solid-Phase Synthesis of Hydantoins p595-599 By Isabelle Parrot ; Isabelle Parrot IBMM UMR 5247 CNRS-Université Montpellier 1 et 2, Faculté des Sciences Pl. Eugène Bataillon 34 095 Montpellier Cedex 5 France [email protected] Search for other works by this author on: This Site PubMed Google Scholar Guilhem Chaubet Guilhem Chaubet IBMM UMR 5247 CNRS-Université Montpellier 1 et 2, Faculté des Sciences Pl. Eugène Bataillon 34 095 Montpellier Cedex 5 France [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 8.2. Microwave-Assisted Solid-Phase Synthesis of Hydantoins in another window
9.1.1. Preparation of Cyclohexene p600-602 By Abel J. S. C. Vieira ; Abel J. S. C. Vieira Faculty of Sciences and Technology, Universidade Nova de Lisboa 2829-516 Caparica Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Elvira M. S. M. Gaspar Elvira M. S. M. Gaspar Faculty of Sciences and Technology, Universidade Nova de Lisboa 2829-516 Caparica Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 9.1.1. Preparation of Cyclohexene in another window
9.1.2. A Green Synthesis of 2,3-Dibromo-3-phenylpropionic Acid and the Use of Kinetic Studies to Probe into the Elimination Product When Treated with a Weak Base in Different Solvents p603-607 By Malcolm I. Stewart ; Malcolm I. Stewart CRL, University of Oxford 12 Mansfield Road Oxford OX1 3TA UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Craig D. Campbell Craig D. Campbell CRL, University of Oxford 12 Mansfield Road Oxford OX1 3TA UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 9.1.2. A Green Synthesis of 2,3-Dibromo-3-phenylpropionic Acid and the Use of Kinetic Studies to Probe into the Elimination Product When Treated with a Weak Base in Different Solvents in another window
9.1.3. Dehydration of Methylcyclohexanols p608-613 By Cornelis A. Van Walree ; Cornelis A. Van Walree Department of Chemistry, Utrecht University Budapestlaan 4b 3584 CD Utrecht The Netherlands School of Chemical and Physical Sciences, Flinders University GPO Box 2100 Adelaide 5001 Australia [email protected] Search for other works by this author on: This Site PubMed Google Scholar Stephan A. Jonker ; Stephan A. Jonker Department of Chemistry, Utrecht University Budapestlaan 4b 3584 CD Utrecht The Netherlands Search for other works by this author on: This Site PubMed Google Scholar Veronica Kaats-Richters Veronica Kaats-Richters Department of Chemistry, Utrecht University Budapestlaan 4b 3584 CD Utrecht The Netherlands Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 9.1.3. Dehydration of Methylcyclohexanols in another window
9.1.4. Synthesis of 5-Hydroxymethylfurfural (HMF) from Fructose as a Bioplatform Intermediate p614-616 By Svilen P. Simeonov ; Svilen P. Simeonov Research Institute for Medicines and Pharmaceuticals Sciences, Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisbon Portugal Institute of Organic Chemistry with Centre of Phytochemistry, Bulgarian Academy of Sciences Acad. G. Bonchev str., bl.9 1113 Sofia Bulgaria [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso Research Institute for Medicines and Pharmaceuticals Sciences, Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisbon Portugal Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 9.1.4. Synthesis of 5-Hydroxymethylfurfural (HMF) from Fructose as a Bioplatform Intermediate in another window
9.2.1. Synthesis of trans -9-(2-Phenylethenyl)anthracene p617-619 By Dulce Simão Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 9.2.1. Synthesis of trans-9-(2-Phenylethenyl)anthracene in another window
9.2.2. Synthesis of 4-Vinylbenzoic acid p620-622 By Dulce Simão ; Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana C. Cerdeira Ana C. Cerdeira Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 9.2.2. Synthesis of 4-Vinylbenzoic acid in another window
9.2.3. Preparation of Nitrostilbenes by the Wittig Reaction p623-626 By Francisca Lopes ; Francisca Lopes Research Institute for Medicines (iMed. ULisboa), Faculdade de Farmácia da, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria de Jesus Perry ; Maria de Jesus Perry Research Institute for Medicines (iMed. ULisboa), Faculdade de Farmácia da, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana Paula Francisco Ana Paula Francisco Research Institute for Medicines (iMed. ULisboa), Faculdade de Farmácia da, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 9.2.3. Preparation of Nitrostilbenes by the Wittig Reaction in another window
9.2.4. Building an Alkene Spacer by the Wittig Reaction: Synthesis of 4-[2-(4-Nitrophenyl)ethenyl]benzonitrile p627-630 By António P. S. Teixeira ; António P. S. Teixeira Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora Rua Romão Ramalho 59 7000-671 Évora Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Paula Robalo ; M. Paula Robalo Área Departamental de Engenharia Química, Instituto Superior de Engenharia de Lisboa Rua Conselheiro Emídio Navarro, 1 1959-007 Lisboa Portugal Centro de Química Estrutural, Complexo I, Instituto Superior Técnico, Universidade de Lisboa Av. Rovisco Pais 1049-001 Lisboa Portugal Search for other works by this author on: This Site PubMed Google Scholar Paulo J. Mendes Paulo J. Mendes Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora Rua Romão Ramalho 59 7000-671 Évora Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 9.2.4. Building an Alkene Spacer by the Wittig Reaction: Synthesis of 4-[2-(4-Nitrophenyl)ethenyl]benzonitrile in another window
9.2.5. Preparation of trans , trans -Distyrylbenzene by a Wittig Reaction p631-634 By Arno Kraft Arno Kraft Heriot-Watt University, Institute of Chemical Sciences, School of Engineering & Physical Sciences Riccarton Edinburgh EH14 4AS United Kingdom [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 9.2.5. Preparation of trans,trans-Distyrylbenzene by a Wittig Reaction in another window
9.2.6. Synthesis and Reactivity of Phosphorus Ylides p635-639 By Ana Lúcia Cardoso ; Ana Lúcia Cardoso Department of Chemistry, University of Coimbra Rua Larga 3004-535 Coimbra Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria I. L. Soares ; Maria I. L. Soares Department of Chemistry, University of Coimbra Rua Larga 3004-535 Coimbra Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Susana M. M. Lopes ; Susana M. M. Lopes Department of Chemistry, University of Coimbra Rua Larga 3004-535 Coimbra Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Teresa M. V. D. Pinho e Melo Teresa M. V. D. Pinho e Melo Department of Chemistry, University of Coimbra Rua Larga 3004-535 Coimbra Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 9.2.6. Synthesis and Reactivity of Phosphorus Ylides in another window
9.2.7. Synthesis of 4-(Thiophen-2-yl)pyrrolidin-2-one via Horner–Wadsworth–Emmons Reaction and Reductive Cyclisation p640-645 By Jonathan D. Sellars ; Jonathan D. Sellars Chemistry Department, University of Durham South Road Durham DH1 3LE UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar AnnMarie C. O’Donoghue ; AnnMarie C. O’Donoghue Chemistry Department, University of Durham South Road Durham DH1 3LE UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ian R. Baxendale ; Ian R. Baxendale Chemistry Department, University of Durham South Road Durham DH1 3LE UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar John M. Sanderson ; John M. Sanderson Chemistry Department, University of Durham South Road Durham DH1 3LE UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Elizabeth J. Grayson Elizabeth J. Grayson Chemistry Department, University of Durham South Road Durham DH1 3LE UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 9.2.7. Synthesis of 4-(Thiophen-2-yl)pyrrolidin-2-one via Horner–Wadsworth–Emmons Reaction and Reductive Cyclisation in another window
9.3.1. A Guided-Inquiry Approach to Ring-Closing Metathesis p646-649 By Hala G. Schepmann ; Hala G. Schepmann Southern Oregon University 1250 Siskiyou Boulevard Ashland Oregon 97520 USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar Michelle Mynderse Michelle Mynderse 2371 Henley Avenue Berkley Michigan 48072 USA Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 9.3.1. A Guided-Inquiry Approach to Ring-Closing Metathesis in another window
9.3.2. Sequential Pd-Catalyzed Allylic Alkylation/Ru-Catalyzed Ring-Closing Metathesis p650-655 By Mélanie M. Lorion ; Mélanie M. Lorion UPMC Univ Paris 06, IPCM UMR CNRS 8232, FR2769, Institut Parisien de Chimie Moléculaire Paris France CNRS, UMR 8232 F-75005 Paris France [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Claire Kammerer ; Claire Kammerer Search for other works by this author on: This Site PubMed Google Scholar Guillaume Prestat ; Guillaume Prestat Search for other works by this author on: This Site PubMed Google Scholar Giovanni Poli Giovanni Poli UPMC Univ Paris 06, IPCM UMR CNRS 8232, FR2769, Institut Parisien de Chimie Moléculaire Paris France CNRS, UMR 8232 F-75005 Paris France [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 9.3.2. Sequential Pd-Catalyzed Allylic Alkylation/Ru-Catalyzed Ring-Closing Metathesis in another window
10.1. Diels–Alder Reaction of N -Phenylmaleimide with In situ Generated Buta-1,3-diene p656-659 By Artur M. S. Silva ; Artur M. S. Silva Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Augusto C. Tomé ; Augusto C. Tomé Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Diana C. G. A. Pinto ; Diana C. G. A. Pinto Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernando Domingues ; Fernando Domingues Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Graça M. Oliveira Rocha ; Graça M. Oliveira Rocha Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar José A. S. Cavaleiro ; José A. S. Cavaleiro Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Graça P. M. S. Neves ; M. Graça P. M. S. Neves Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Amparo F. Faustino ; M. Amparo F. Faustino Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Mário M. Q. Simões Mário M. Q. Simões Department of Chemistry and QOPNA, University of Aveiro 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 10.1. Diels–Alder Reaction of N-Phenylmaleimide with In situ Generated Buta-1,3-diene in another window
10.2. Synthesis of Isomeric Bicyclopropyls from Conjugated Dienes p660-663 By Leiv K. Sydnes ; Leiv K. Sydnes Department of Chemistry Allégt. 41 5007 Bergen Norway [email protected] Search for other works by this author on: This Site PubMed Google Scholar Magne O. Sydnes Magne O. Sydnes Faculty of Science and Technology, Department of Mathematics and Natural Science 4036 Stavanger Norway Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 10.2. Synthesis of Isomeric Bicyclopropyls from Conjugated Dienes in another window
10.3. Diels–Alder Reaction Between p -Benzoquinone and Cyclopentadiene and Subsequent Photochemical [2π + 2π] Cycloaddition p664-667 By Arno Kraft Arno Kraft Heriot-Watt University, Institute of Chemical Sciences, School of Engineering & Physical Sciences Riccarton, Edinburgh EH14 4AS United Kingdom [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 10.3. Diels–Alder Reaction Between p-Benzoquinone and Cyclopentadiene and Subsequent Photochemical [2π + 2π] Cycloaddition in another window
10.4. Click Chemistry p668-670 By Susana Dias Lucas ; Susana Dias Lucas Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Eduardo F. P. Ruivo ; Eduardo F. P. Ruivo Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Marta Figueiras ; Marta Figueiras Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar João P. Lavrado ; João P. Lavrado Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Rui Moreira Rui Moreira Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 10.4. Click Chemistry in another window
10.5. On-Water Synthesis of a Dipyrromethane via Bis-hetero-Diels–Alder Reaction of an Azoalkene with Pyrrole p671-675 By Susana M. M. Lopes ; Susana M. M. Lopes Department of Chemistry, University of Coimbra Rua Larga 3004-535 Coimbra Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria I. L. Soares ; Maria I. L. Soares Department of Chemistry, University of Coimbra Rua Larga 3004-535 Coimbra Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana Lúcia Cardoso ; Ana Lúcia Cardoso Department of Chemistry, University of Coimbra Rua Larga 3004-535 Coimbra Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Américo Lemos ; Américo Lemos CIQA, FCT, University of Algarve, Campus de Gambelas 8005-139 Faro Portugal Search for other works by this author on: This Site PubMed Google Scholar Teresa M. V. D. Pinho e Melo Teresa M. V. D. Pinho e Melo Department of Chemistry, University of Coimbra Rua Larga 3004-535 Coimbra Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 10.5. On-Water Synthesis of a Dipyrromethane via Bis-hetero-Diels–Alder Reaction of an Azoalkene with Pyrrole in another window
10.6. Application of 2,4,6-Trioxo-pyrimidin-5-ylidene Alditol in the Synthesis of Pyrano[2,3- d ]pyrimidine Containing a Sugar Moiety by Hetero-Diels–Alder Reaction p676-680 By Aleksandra Pałasz ; Aleksandra Pałasz Department of Organic Chemistry, Faculty of Chemistry, Jagiellonian University Ingardena 3 St 30-060 Kraków Poland [email protected] Search for other works by this author on: This Site PubMed Google Scholar Dariusz Cież Dariusz Cież Department of Organic Chemistry, Faculty of Chemistry, Jagiellonian University Ingardena 3 St 30-060 Kraków Poland [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 10.6. Application of 2,4,6-Trioxo-pyrimidin-5-ylidene Alditol in the Synthesis of Pyrano[2,3-d]pyrimidine Containing a Sugar Moiety by Hetero-Diels–Alder Reaction in another window
10.7. Synthesis of a Spiroisoxazoline Oxindole by 1,3-Dipolar Cycloaddition p681-684 By Carlos J. A. Ribeiro ; Carlos J. A. Ribeiro Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Professor Gama Pinto 1649-003 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Rui Moreira ; Rui Moreira Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Professor Gama Pinto 1649-003 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria M. M. Santos Maria M. M. Santos Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Professor Gama Pinto 1649-003 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 10.7. Synthesis of a Spiroisoxazoline Oxindole by 1,3-Dipolar Cycloaddition in another window
10.8. Oxonitriles: Four-Step Ozonolysis, Aldol, Conjugate Addition, and Enolate Acylation Sequence p685-689 By Jesus A. Lujan-Montelongo ; Jesus A. Lujan-Montelongo Departamento de Química, Centro de Investigación y de Estudios Avanzados (Cinvestav), Avenida Instituto Politécnico Nacional 2508 San Pedro Zacatenco 07360 México D. F. Mexico Search for other works by this author on: This Site PubMed Google Scholar Fraser F. Fleming Fraser F. Fleming Department of Chemistry, Drexel University 32 South 32nd St. Philadelphia PA 19104 USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 10.8. Oxonitriles: Four-Step Ozonolysis, Aldol, Conjugate Addition, and Enolate Acylation Sequence in another window
10.9. Flash Vacuum Pyrolysis of o -Phenylene Sulfite: Formation and Purification of Cyclopentadienone Dimer p690-693 By R. Alan Aitken ; R. Alan Aitken EaStCHEM School of Chemistry, University of St Andrews North Haugh, St Andrews Fife KY16 9ST UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Caroline E. R. Horsburgh Caroline E. R. Horsburgh EaStCHEM School of Chemistry, University of St Andrews North Haugh, St Andrews Fife KY16 9ST UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 10.9. Flash Vacuum Pyrolysis of o-Phenylene Sulfite: Formation and Purification of Cyclopentadienone Dimer in another window
11.1. Synthesis of 4-Methoxymethylbenzoic Acid p694-696 By Dulce Simão ; Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana C. Cerdeira Ana C. Cerdeira Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 11.1. Synthesis of 4-Methoxymethylbenzoic Acid in another window
11.2. Synthesis of Benzopinacolone via Benzophenone Photoreduction Followed by Pinacol Rearrangement p697-700 By Filipa Siopa ; Filipa Siopa iMed.ULisboa Av. Professor Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso iMed.ULisboa Av. Professor Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 11.2. Synthesis of Benzopinacolone via Benzophenone Photoreduction Followed by Pinacol Rearrangement in another window
11.3. Iodosulfonylation–Dehydroiodination of Styrene: Synthesis of ( E )-β-Tosylstyrene p701-703 By Carmen Nájera ; Carmen Nájera Departamento de Química Orgánica and Centro de Innovación en Química Avanzada (ORFEO-CINQA). Universidad de Alicante Ctra. San Vicente s/n E-03690-San Vicente del Raspeig (Alicante) Spain [email protected] Search for other works by this author on: This Site PubMed Google Scholar José M. Sansano ; José M. Sansano Departamento de Química Orgánica and Centro de Innovación en Química Avanzada (ORFEO-CINQA). Universidad de Alicante Ctra. San Vicente s/n E-03690-San Vicente del Raspeig (Alicante) Spain [email protected] Search for other works by this author on: This Site PubMed Google Scholar Miguel Yus Miguel Yus Departamento de Química Orgánica and Centro de Innovación en Química Avanzada (ORFEO-CINQA). Universidad de Alicante Ctra. San Vicente s/n E-03690-San Vicente del Raspeig (Alicante) Spain [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 11.3. Iodosulfonylation–Dehydroiodination of Styrene: Synthesis of (E)-β-Tosylstyrene in another window
12.1.1. Aerobic Alcohol Oxidation Using a Cu( i )/TEMPO Catalyst System p704-708 By Nicholas J. Hill ; Nicholas J. Hill Department of Chemistry, University of Wisconsin-Madison 1101 University Avenue Madison WI 53706 USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar Jessica M. Hoover ; Jessica M. Hoover Department of Chemistry, University of Wisconsin-Madison 1101 University Avenue Madison WI 53706 USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar Shannon S. Stahl Shannon S. Stahl Department of Chemistry, University of Wisconsin-Madison 1101 University Avenue Madison WI 53706 USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.1.1. Aerobic Alcohol Oxidation Using a Cu(i)/TEMPO Catalyst System in another window
12.1.2. Chemoselective Oxidation of 1,2-Tetradecanediol p709-712 By Siedlecka Renata ; Siedlecka Renata Faculty of Chemistry, Organic Chemistry Department, Wroclaw University of Technology Wyb. Wyspianskiego 27 50-370 Wroclaw Poland [email protected] Search for other works by this author on: This Site PubMed Google Scholar Skarżewski Jacek Skarżewski Jacek Faculty of Chemistry, Organic Chemistry Department, Wroclaw University of Technology Wyb. Wyspianskiego 27 50-370 Wroclaw Poland [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.1.2. Chemoselective Oxidation of 1,2-Tetradecanediol in another window
12.1.3. Catalyzed Oxidation of Naphthalene to 1,4-Naphthoquinone p713-715 By Jacek Skarżewski Jacek Skarżewski Department of Organic Chemistry, Wroclaw University of Technology Wyb. Wyspianskiego 27 50-370 Wroclaw Poland [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.1.3. Catalyzed Oxidation of Naphthalene to 1,4-Naphthoquinone in another window
12.1.4. Alcohol Oxidation: Menthone Preparation by Menthol Oxidation Using Pyridinium Chlorochromate Immobilized in Silica Gel p716-719 By Rafael F. A. Gomes ; Rafael F. A. Gomes iMed.UL, Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso iMed.UL, Faculty of Pharmacy, University of Lisbon Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.1.4. Alcohol Oxidation: Menthone Preparation by Menthol Oxidation Using Pyridinium Chlorochromate Immobilized in Silica Gel in another window
12.1.5. Heterocyclic Target Synthesis – Three-Step Syntheses from Benzaldehyde p720-724 By Iain A. Smellie ; Iain A. Smellie School of Chemistry, University of St Andrews North Haugh, St Andrews Fife KY16 9ST UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Nigel P. Botting ; Nigel P. Botting School of Chemistry, University of St Andrews North Haugh, St Andrews Fife KY16 9ST UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Brian A. Chalmers ; Brian A. Chalmers School of Chemistry, University of St Andrews North Haugh, St Andrews Fife KY16 9ST UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Andrew D. Harper ; Andrew D. Harper School of Chemistry, University of St Andrews North Haugh, St Andrews Fife KY16 9ST UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Iain L. J. Patterson Iain L. J. Patterson School of Chemistry, University of St Andrews North Haugh, St Andrews Fife KY16 9ST UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.1.5. Heterocyclic Target Synthesis – Three-Step Syntheses from Benzaldehyde in another window
12.1.6. Oxidation of Activated Phenols p725-729 By Luísa M. Ferreira ; Luísa M. Ferreira LAQV, REQUIMTE, Departamento de Química, Faculdade de Ciências e Tecnologia, Universidade Nova de Lisboa Campus da Caparica Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Paula S. Branco Paula S. Branco LAQV, REQUIMTE, Departamento de Química, Faculdade de Ciências e Tecnologia, Universidade Nova de Lisboa Campus da Caparica Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.1.6. Oxidation of Activated Phenols in another window
12.2.1. Synthesis of 2-(5-Phenylthien-2′-yl)benzothiazole p730-732 By Maria Manuela Marques Raposo ; Maria Manuela Marques Raposo Department of Chemistry, University of Minho Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Susana Paula Graça da Costa ; Susana Paula Graça da Costa Department of Chemistry, University of Minho Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Rosa Maria Ferreira Batista Rosa Maria Ferreira Batista Department of Chemistry, University of Minho Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.2.1. Synthesis of 2-(5-Phenylthien-2′-yl)benzothiazole in another window
12.2.2. Synthesis of N - tert -butyloxycarbonyl-[2-(thien-2′-yl)benzoxazol-5-yl]- l -alanine methyl ester p733-736 By Susana P. G. Costa ; Susana P. G. Costa Department of Chemistry, University of Minho Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Manuela M. Raposo ; M. Manuela M. Raposo Department of Chemistry, University of Minho Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Cátia I. C. Esteves ; Cátia I. C. Esteves Department of Chemistry, University of Minho Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar R. Cristina M. Ferreira R. Cristina M. Ferreira Department of Chemistry, University of Minho Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.2.2. Synthesis of N-tert-butyloxycarbonyl-[2-(thien-2′-yl)benzoxazol-5-yl]-l-alanine methyl ester in another window
12.2.3. Synthesis of Flavones (2-Aryl-4 H -chromen-4-ones) p737-740 By Artur M. S. Silva ; Artur M. S. Silva Chemistry Department & QOPNA, University of Aveiro Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Augusto C. Tomé ; Augusto C. Tomé Chemistry Department & QOPNA, University of Aveiro Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Diana C. G. A. Pinto ; Diana C. G. A. Pinto Chemistry Department & QOPNA, University of Aveiro Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernando Domingues ; Fernando Domingues Chemistry Department & QOPNA, University of Aveiro Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Graça M. Oliveira Rocha ; Graça M. Oliveira Rocha Chemistry Department & QOPNA, University of Aveiro Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar José A. S. Cavaleiro ; José A. S. Cavaleiro Chemistry Department & QOPNA, University of Aveiro Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Graça P. M. S. Neves ; M. Graça P. M. S. Neves Chemistry Department & QOPNA, University of Aveiro Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Amparo F. Faustino ; M. Amparo F. Faustino Chemistry Department & QOPNA, University of Aveiro Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Mário M. Q. Simões Mário M. Q. Simões Chemistry Department & QOPNA, University of Aveiro Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.2.3. Synthesis of Flavones (2-Aryl-4H-chromen-4-ones) in another window
12.2.4. Hantzsch Synthesis of 3,5-Diethoxycarbonyl-2,6-dimethylpyridine p741-744 By Iain A. Smellie ; Iain A. Smellie School of Chemistry, University of St Andrews North Haugh, St Andrews Fife KY16 9ST UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Nigel P. Botting ; Nigel P. Botting School of Chemistry, University of St Andrews North Haugh, St Andrews Fife KY16 9ST UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Brian A. Chalmers ; Brian A. Chalmers School of Chemistry, University of St Andrews North Haugh, St Andrews Fife KY16 9ST UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Iain L. J. Patterson ; Iain L. J. Patterson School of Chemistry, University of St Andrews North Haugh, St Andrews Fife KY16 9ST UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Catherine M. Schofield Catherine M. Schofield School of Chemistry, University of St Andrews North Haugh, St Andrews Fife KY16 9ST UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.2.4. Hantzsch Synthesis of 3,5-Diethoxycarbonyl-2,6-dimethylpyridine in another window
12.2.5. An “Out-of-the-Box” Example in Heterocyclic Chemistry: Synthesis of 3,6-Bis-(3,5-dimethyl-1 H -pyrazol-1-yl)-1,2,4,5-tetrazine p745-749 By Tiago J. L. Silva ; Tiago J. L. Silva Centro de Química Estrutural, Faculdade de Ciências da, Universidade de Lisboa Campo Grande, 1049-1016 Campo Grande, Lisboa Portugal Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora Rua Romão Ramalho 59 7000-671 Évora Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Paulo J. G. Mendes ; Paulo J. G. Mendes Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora Rua Romão Ramalho 59 7000-671 Évora Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana Isabel Tomaz ; Ana Isabel Tomaz Centro de Química Estrutural, Faculdade de Ciências da, Universidade de Lisboa Campo Grande, 1049-1016 Campo Grande, Lisboa Portugal Search for other works by this author on: This Site PubMed Google Scholar M. Helena Garcia M. Helena Garcia Centro de Química Estrutural, Faculdade de Ciências da, Universidade de Lisboa Campo Grande, 1049-1016 Campo Grande, Lisboa Portugal Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.2.5. An “Out-of-the-Box” Example in Heterocyclic Chemistry: Synthesis of 3,6-Bis-(3,5-dimethyl-1H-pyrazol-1-yl)-1,2,4,5-tetrazine in another window
12.3.1. Catalytic Epoxidation of cis -Cyclooctene with MTO( vii ) and Pyrazole p750-753 By Elisabete P. Carreiro ; Elisabete P. Carreiro Centro de Química de Évora, Institute for Research and Advanced Studies, University of Evora, Chemistry Department, School of Science and Technology Rua Romão Ramalho, no. 59 7000-671 Évora Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Anthony J. Burke Anthony J. Burke Centro de Química de Évora, Institute for Research and Advanced Studies, University of Evora, Chemistry Department, School of Science and Technology Rua Romão Ramalho, no. 59 7000-671 Évora Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.3.1. Catalytic Epoxidation of cis-Cyclooctene with MTO(vii) and Pyrazole in another window
12.3.2. Stereoselective Epoxidation of Cholesterol by m -Chloroperoxybenzoic Acid p754-757 By Maria de Jesus Perry ; Maria de Jesus Perry Instituto de Investigação do Medicamento (iMed. ULisboa), Faculdade de Farmácia da Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana Paula Francisco ; Ana Paula Francisco Instituto de Investigação do Medicamento (iMed. ULisboa), Faculdade de Farmácia da Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana S. Ressurreição ; Ana S. Ressurreição Instituto de Investigação do Medicamento (iMed. ULisboa), Faculdade de Farmácia da Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Francisca Lopes Francisca Lopes Instituto de Investigação do Medicamento (iMed. ULisboa), Faculdade de Farmácia da Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.3.2. Stereoselective Epoxidation of Cholesterol by m-Chloroperoxybenzoic Acid in another window
12.3.3. Green Oxidation of Organic Compounds Using Metalloporphyrins p758-761 By Rose A. Clark ; Rose A. Clark Department of Chemistry, Saint Francis University Loretto PA 15940 USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar Anne E. Stock ; Anne E. Stock Department of Chemistry, Saint Francis University Loretto PA 15940 USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar Edward P. Zovinka Edward P. Zovinka Department of Chemistry, Saint Francis University Loretto PA 15940 USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.3.3. Green Oxidation of Organic Compounds Using Metalloporphyrins in another window
12.3.4. Catalytic Epoxidation of Carbamazepine p762-765 By Artur M. S. Silva ; Artur M. S. Silva Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Augusto C. Tomé ; Augusto C. Tomé Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Diana C. G. A. Pinto ; Diana C. G. A. Pinto Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernando M. J. Domingues ; Fernando M. J. Domingues Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Graça M. S. R. O. Rocha ; Graça M. S. R. O. Rocha Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar José A. S. Cavaleiro ; José A. S. Cavaleiro Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria da Graça P. M. S. Neves ; Maria da Graça P. M. S. Neves Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria do Amparo F. Faustino ; Maria do Amparo F. Faustino Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Mário M. Q. Simões Mário M. Q. Simões Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.3.4. Catalytic Epoxidation of Carbamazepine in another window
12.3.5. Regioselective Epoxidation of Geraniol by VO(acac) 2 Immobilised in Polystyrene p766-768 By Ana I. Vicente ; Ana I. Vicente iMed.ULisboa, Faculdade de Farmácia da Universidade de Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso iMed.ULisboa, Faculdade de Farmácia da Universidade de Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.3.5. Regioselective Epoxidation of Geraniol by VO(acac)2 Immobilised in Polystyrene in another window
12.3.6. Organocatalysed trans -Dihydroxylation of Olefins p769-772 By Andreia A. Rosatella ; Andreia A. Rosatella iMed.ULisboa, Faculdade de Farmácia da Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso iMed.ULisboa, Faculdade de Farmácia da Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.3.6. Organocatalysed trans-Dihydroxylation of Olefins in another window
12.4.1. Synthesis of 6-Nitrosaccharin p773-775 By Dulce Simão ; Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana C. Cerdeira Ana C. Cerdeira Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 12.4.1. Synthesis of 6-Nitrosaccharin in another window
13.1. Reduction of a Ketone Using Sodium Borohydride. Control of a Reaction by TLC p776-780 By Luis Constantino ; Luis Constantino Faculty of Pharmacy, Universidade de Lisboa Av. Professor Gama Pinto 1649-003 Lisbon Portugal Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Professor Gama Pinto 1649-003 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Catarina Dias ; Catarina Dias Faculty of Pharmacy, Universidade de Lisboa Av. Professor Gama Pinto 1649-003 Lisbon Portugal Search for other works by this author on: This Site PubMed Google Scholar Emília Valente Emília Valente Faculty of Pharmacy, Universidade de Lisboa Av. Professor Gama Pinto 1649-003 Lisbon Portugal Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 13.1. Reduction of a Ketone Using Sodium Borohydride. Control of a Reaction by TLC in another window
13.2. Regioselective Catalytic Transfer Hydrogenation of Citral p781-783 By Jaime A. S. Coelho ; Jaime A. S. Coelho iMed.UL, Faculdade de Farmácia da Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso iMed.UL, Faculdade de Farmácia da Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 13.2. Regioselective Catalytic Transfer Hydrogenation of Citral in another window
13.3. Regioselective 1,2-Reduction of an α,β-Unsaturated Ketone. A Green Experiment p784-788 By M. Manuela A. Pereira M. Manuela A. Pereira REQUIMTE, Chemistry Department, Faculdade de Ciências e Tecnologia, Universidade Nova de Lisboa 2827-516 Caparica Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 13.3. Regioselective 1,2-Reduction of an α,β-Unsaturated Ketone. A Green Experiment in another window
13.4. Reduction of Diphenyl Sulfoxide Catalyzed by the Dioxo-Molybdenum Complex MoO 2 Cl 2 (H 2 O) 2 p789-793 By Ana C. Fernandes ; Ana C. Fernandes Centro de Química Estrutural, Instituto Superior Técnico, Universidade de Lisboa Av. Rovisco Pais, 1 1049-001 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Tiago A. Fernandes Tiago A. Fernandes Centro de Química Estrutural, Instituto Superior Técnico, Universidade de Lisboa Av. Rovisco Pais, 1 1049-001 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 13.4. Reduction of Diphenyl Sulfoxide Catalyzed by the Dioxo-Molybdenum Complex MoO2Cl2(H2O)2 in another window
13.5. Synthesis of Allylic Esters by Reduction of Fructone Followed by Wittig Olefination p794-797 By Thomas A. Logothetis Thomas A. Logothetis University of Southampton, Chemistry Highfield, Southampton Hampshire SO17 1BJ UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 13.5. Synthesis of Allylic Esters by Reduction of Fructone Followed by Wittig Olefination in another window
13.6. Preparation of a Thia-Tetraaza Macrocyclic Compound Through a Dual-Step Synthesis p798-802 By Judite Costa ; Judite Costa Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Professor Gama Pinto 1649-003 Lisbon Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar João Franco Machado ; João Franco Machado Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Professor Gama Pinto 1649-003 Lisbon Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Fátima Cabral M. Fátima Cabral Research Institute for Medicines (iMed.ULisboa), Faculty of Pharmacy, Universidade de Lisboa Av. Professor Gama Pinto 1649-003 Lisbon Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 13.6. Preparation of a Thia-Tetraaza Macrocyclic Compound Through a Dual-Step Synthesis in another window
13.7. Asymmetric Reduction of Acetophenone with Borane Catalyzed by B -Methoxy-oxazaborolidine p803-806 By Marek P. Krzemiński Marek P. Krzemiński Department of Organic Chemistry, Faculty of Chemistry, Nicolaus Copernicus, University in Toruń Poland [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 13.7. Asymmetric Reduction of Acetophenone with Borane Catalyzed by B-Methoxy-oxazaborolidine in another window
13.8. Synthesis of 4,5-Bis(benzoylthio)-1,3-dithiole-2-thione p807-810 By Dulce Simão ; Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais 1, 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana C. Cerdeira Ana C. Cerdeira Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais 1, 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 13.8. Synthesis of 4,5-Bis(benzoylthio)-1,3-dithiole-2-thione in another window
13.9. Organocatalytic Asymmetric Reduction of ( E )- N ,1-Diphenyl-1-propanimine to N -(1-Phenylpropyl)aniline with Trichlorosilane p811-814 By Pedro Barrulas ; Pedro Barrulas Departamento de Química e Centro de Química de Évora, Universidade de Évora Rua Romão Ramalho, 59 7000 Évora Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Anthony Burke Anthony Burke Departamento de Química e Centro de Química de Évora, Universidade de Évora Rua Romão Ramalho, 59 7000 Évora Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 13.9. Organocatalytic Asymmetric Reduction of (E)-N,1-Diphenyl-1-propanimine to N-(1-Phenylpropyl)aniline with Trichlorosilane in another window
14.1. Benzilic Acid Rearrangement p815-817 By Paulo Coelho ; Paulo Coelho Centro de Química – Vila Real, Universidade de Trás-os-Montes e Alto Douro 5001-801 Vila Real Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Céu Sousa Céu Sousa Centro de Química – Vila Real, Universidade de Trás-os-Montes e Alto Douro 5001-801 Vila Real Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 14.1. Benzilic Acid Rearrangement in another window
14.2. Preparation of Phenyl Acetate and Its Conversion into 4-Hydroxyacetophenone p818-820 By Eimíle Sheehy ; Eimíle Sheehy Center for Synthesis and Chemical Biology, School of Chemistry, University College Dublin Dublin 4 Ireland [email protected] Search for other works by this author on: This Site PubMed Google Scholar Paul Evans Paul Evans Center for Synthesis and Chemical Biology, School of Chemistry, University College Dublin Dublin 4 Ireland [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 14.2. Preparation of Phenyl Acetate and Its Conversion into 4-Hydroxyacetophenone in another window
14.3. Multistep Synthesis of Dilantin p821-825 By Paula C. Castilho ; Paula C. Castilho CQM, Centro de Competências de Ciências Exactas e das Engenharias, Universidade da Madeira, Campus Universitário da Penteada 9020-105 Funchal Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Pedro Ideia Pedro Ideia CQM, Centro de Competências de Ciências Exactas e das Engenharias, Universidade da Madeira, Campus Universitário da Penteada 9020-105 Funchal Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 14.3. Multistep Synthesis of Dilantin in another window
14.4. Preparation of Isoborneol Through the Wagner–Meerwein Rearrangement Reaction of (1 R )-(+)-Camphene p826-829 By Marek P. Krzemiński Marek P. Krzemiński Department of Organic Chemistry, Faculty of Chemistry, Nicolaus Copernicus University in Toruń Poland [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 14.4. Preparation of Isoborneol Through the Wagner–Meerwein Rearrangement Reaction of (1R)-(+)-Camphene in another window
14.5. Umbelliferone: A Natural Scaffold Suitable for the Synthesis of ortho -Acetylhydroxycoumarins via Fries Rearrangement Reaction p830-833 By Saleta Vazquez-Rodriguez ; Saleta Vazquez-Rodriguez CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences, University of Porto Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria João Matos ; Maria João Matos CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences, University of Porto Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Eugenio Uriarte ; Eugenio Uriarte Department of Organic Chemistry, Faculty of Pharmacy, University of Santiago de Compostela Spain Search for other works by this author on: This Site PubMed Google Scholar Lourdes Santana ; Lourdes Santana Department of Organic Chemistry, Faculty of Pharmacy, University of Santiago de Compostela Spain Search for other works by this author on: This Site PubMed Google Scholar Fernanda Borges Fernanda Borges CIQUP/Department of Chemistry and Biochemistry, Faculty of Sciences, University of Porto Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 14.5. Umbelliferone: A Natural Scaffold Suitable for the Synthesis of ortho-Acetylhydroxycoumarins via Fries Rearrangement Reaction in another window
14.6. Preparation of 4,5-Functionalized Cyclopentenone via Cyclization of a Stenhouse Adduct p834-837 By Jaime A. S. Coelho ; Jaime A. S. Coelho iMed.UL, Faculdade de Farmácia da Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso iMed.UL, Faculdade de Farmácia da Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 14.6. Preparation of 4,5-Functionalized Cyclopentenone via Cyclization of a Stenhouse Adduct in another window
14.7. Synthesis of a Chiral Salen. Examples of the Schmidt Rearrangement and Ultrasound Activation p838-840 By Maria Elisa da Silva Serra ; Maria Elisa da Silva Serra Department of Chemistry, University of Coimbra Coimbra Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Dina Maria Bairrada Murtinho Dina Maria Bairrada Murtinho Department of Chemistry, University of Coimbra Coimbra Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 14.7. Synthesis of a Chiral Salen. Examples of the Schmidt Rearrangement and Ultrasound Activation in another window
15.1. Bioreduction of N -Oxide Moiety p841-846 By María Laura Lavaggi ; María Laura Lavaggi Laboratorio de Química Orgánica, Instituto de Química Biológica, Facultad de Ciencias, Universidad de la República Iguá 4225 Montevideo 11400 Uruguay [email protected] Search for other works by this author on: This Site PubMed Google Scholar Mercedes González ; Mercedes González Laboratorio de Química Orgánica, Instituto de Química Biológica, Facultad de Ciencias, Universidad de la República Iguá 4225 Montevideo 11400 Uruguay [email protected] Search for other works by this author on: This Site PubMed Google Scholar Hugo Cerecetto Hugo Cerecetto Área de Radiofarmacia, Centro de Investigaciones Nucleares, Facultad de Ciencias, Universidad de la República Mataojo 2055 Montevideo 11400 Uruguay [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 15.1. Bioreduction of N-Oxide Moiety in another window
16.1. Preparation of Nylon 6,6 by Interfacial Polymerization p847-848 By João P. Telo João P. Telo Centro de Química Estrutural, Instituto Superior Técnico, Universidade de Lisboa Av. Rovisco Pais 1649-003 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 16.1. Preparation of Nylon 6,6 by Interfacial Polymerization in another window
16.2. Synthesis of Copolymer from Acrylamide (AA), 2-Acrylamido-2-methylpropane-sulfonic Acid (AMPS) and N , N -Methyleno-bis-acrylamide (BA) p849-852 By Fátima Coelho ; Fátima Coelho Department of Chemistry, Instituto Superior Técnico, University of Lisbon, CERENA-Centro de Recursos Naturais e Ambiente Av. Rovisco Pais, 1 1049-001 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Dulce Simão Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisboa Portugal Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 16.2. Synthesis of Copolymer from Acrylamide (AA), 2-Acrylamido-2-methylpropane-sulfonic Acid (AMPS) and N,N-Methyleno-bis-acrylamide (BA) in another window
16.3. Multi-Step Synthesis of Nylon from Cyclohexene p853-858 By Marisa G. Weaver ; Marisa G. Weaver University of California at Santa Barbara, Department of Chemistry & Biochemistry 9510, Santa Barbara California 93106-9510 USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar Morgan J. Gainer Morgan J. Gainer University of California at Santa Barbara, Department of Chemistry & Biochemistry 9510, Santa Barbara California 93106-9510 USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 16.3. Multi-Step Synthesis of Nylon from Cyclohexene in another window
16.4. Copolymerisation of Styrene and Methyl Methacrylate: An Introduction to Radical Polymerisation and Monomer Reactivity Ratios p859-863 By Valeria Arrighi ; Valeria Arrighi Heriot-Watt University, Institute of Chemical Sciences, School of Engineering & Physical Sciences Riccarton Edinburgh EH14 4AS UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Arno Kraft Arno Kraft Heriot-Watt University, Institute of Chemical Sciences, School of Engineering & Physical Sciences Riccarton Edinburgh EH14 4AS UK [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 16.4. Copolymerisation of Styrene and Methyl Methacrylate: An Introduction to Radical Polymerisation and Monomer Reactivity Ratios in another window
16.5. Polymerization of ε-Caprolactone Using a Ruthenium( ii ) Mixed Metallocene Catalyst p864-867 By Andreia Valente ; Andreia Valente Centro de Química Estrutural, Faculdade de Ciências da Universidade de Lisboa Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Tiago J. L. Silva ; Tiago J. L. Silva Centro de Química Estrutural, Faculdade de Ciências da Universidade de Lisboa Lisboa Portugal [email protected] Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora Évora Portugal Search for other works by this author on: This Site PubMed Google Scholar Paulo J. G. Mendes ; Paulo J. G. Mendes Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora Évora Portugal Search for other works by this author on: This Site PubMed Google Scholar Ana Isabel Tomaz ; Ana Isabel Tomaz Centro de Química Estrutural, Faculdade de Ciências da Universidade de Lisboa Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Helena Garcia M. Helena Garcia Centro de Química Estrutural, Faculdade de Ciências da Universidade de Lisboa Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 16.5. Polymerization of ε-Caprolactone Using a Ruthenium(ii) Mixed Metallocene Catalyst in another window
17.1. The Cannizzaro Reaction: Synthesis of p -Chlorobenzyl Alcohol and p -Chlorobenzoic Acid p868-870 By Marja Asp-Lehtinen Marja Asp-Lehtinen Department of Chemistry and Bioengineering, Tampere University of Technology P.O. Box 541 33101 Tampere Finland [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 17.1. The Cannizzaro Reaction: Synthesis of p-Chlorobenzyl Alcohol and p-Chlorobenzoic Acid in another window
17.2. The Kemp Elimination in Water: A Laboratory Experiment for Introductory Organic Chemistry p871-874 By Caitlin Williamson ; Caitlin Williamson Department of Chemistry and Biochemistry, Wilfrid Laurier University 75 University Ave W. Waterloo Ontario Canada N2L 3C5 [email protected] Search for other works by this author on: This Site PubMed Google Scholar Kenneth E. Maly ; Kenneth E. Maly Department of Chemistry and Biochemistry, Wilfrid Laurier University 75 University Ave W. Waterloo Ontario Canada N2L 3C5 [email protected] Search for other works by this author on: This Site PubMed Google Scholar Stephen L. MacNeil Stephen L. MacNeil Department of Chemistry and Biochemistry, Wilfrid Laurier University 75 University Ave W. Waterloo Ontario Canada N2L 3C5 [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 17.2. The Kemp Elimination in Water: A Laboratory Experiment for Introductory Organic Chemistry in another window
17.3. Synthesis of Veratronitrile p875-877 By Dulce Simão ; Dulce Simão Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Ana C. Cerdeira Ana C. Cerdeira Department of Chemistry, Instituto Superior Técnico, University of Lisbon, Centro de Química Estrutural Av. Rovisco Pais, 1 1049-001 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 17.3. Synthesis of Veratronitrile in another window
17.4. Synthesis of Levulinic Acid from Sucrose p878-880 By João P. Telo João P. Telo Centro de Química Estrutural, Instituto Superior Técnico, Universidade de Lisboa Av. Rovisco Pais 1049-001 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 17.4. Synthesis of Levulinic Acid from Sucrose in another window
17.5. Synthesis of 1-(4-Bromophenyl)-1 H -pyrrole by the Clauson-Kaas Reaction p881-884 By Maria Manuela Marques Raposo ; Maria Manuela Marques Raposo University of Minho, Department of Chemistry, Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria Cidália Rodrigues Castro ; Maria Cidália Rodrigues Castro University of Minho, Department of Chemistry, Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Sara Sofia Marques Fernandes Sara Sofia Marques Fernandes University of Minho, Department of Chemistry, Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 17.5. Synthesis of 1-(4-Bromophenyl)-1H-pyrrole by the Clauson-Kaas Reaction in another window
17.6. Synthesis of the Manganese( iii ) Complex of 5,10,15,20-Tetrakis(2,6-dichlorophenyl)porphyrin p885-887 By Artur M. S. Silva ; Artur M. S. Silva Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Augusto C. Tomé ; Augusto C. Tomé Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Diana C. G. A. Pinto ; Diana C. G. A. Pinto Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Fernando M. J. Domingues ; Fernando M. J. Domingues Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Graça M. S. R. O. Rocha ; Graça M. S. R. O. Rocha Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar José A. S. Cavaleiro ; José A. S. Cavaleiro Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria da Graça P. M. S. Neves ; Maria da Graça P. M. S. Neves Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Maria do Amparo F. Faustino ; Maria do Amparo F. Faustino Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Mário M. Q. Simões Mário M. Q. Simões Chemistry Department, University of Aveiro, Campus de Santiago 3810-193 Aveiro Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 17.6. Synthesis of the Manganese(iii) Complex of 5,10,15,20-Tetrakis(2,6-dichlorophenyl)porphyrin in another window
17.7. Synthesis of 1,3-Dithienylbenzo[ c ]thiophene p888-892 By Tiago J. L. Silva ; Tiago J. L. Silva Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora Rua Romão Ramalho 59 7000-671 Évora Portugal Centro de Química Estrutural, Faculdade de Ciências da Universidade de Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Paulo J. G. Mendes ; Paulo J. G. Mendes Departamento de Química, Escola de Ciências e Tecnologia, Centro de Química de Évora, Instituto de Investigação e Formação Avançada, Universidade de Évora Rua Romão Ramalho 59 7000-671 Évora Portugal Search for other works by this author on: This Site PubMed Google Scholar Ana Isabel Tomaz ; Ana Isabel Tomaz Centro de Química Estrutural, Faculdade de Ciências da Universidade de Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar M. Helena Garcia M. Helena Garcia Centro de Química Estrutural, Faculdade de Ciências da Universidade de Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 17.7. Synthesis of 1,3-Dithienylbenzo[c]thiophene in another window
17.8. Synthesis of 1-Propyl-2-(thiophen-2-yl)-1 H -pyrrole p893-897 By M. Manuela M. Raposo M. Manuela M. Raposo Department of Chemistry, University of Minho, Campus de Gualtar 4710-057 Braga Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 17.8. Synthesis of 1-Propyl-2-(thiophen-2-yl)-1H-pyrrole in another window
17.9. Rhodium Carbene C–H Insertion in Water and Catalyst Reuse p898-902 By Nuno R. Candeias ; Nuno R. Candeias Tampere University of Technology, Department of Chemistry and Bioengineering Korkeakoulunkatu 8 Tampere FI-33101 Finland [email protected] Search for other works by this author on: This Site PubMed Google Scholar Pedro M. P. Gois ; Pedro M. P. Gois University of Lisbon, Research Institute for Medicines and Pharmaceutical Sciences (iMed.UL), Faculty of Pharmacy Av. Prof. Gama Pinto 1649-003 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso University of Lisbon, Research Institute for Medicines and Pharmaceutical Sciences (iMed.UL), Faculty of Pharmacy Av. Prof. Gama Pinto 1649-003 Lisbon Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 17.9. Rhodium Carbene C–H Insertion in Water and Catalyst Reuse in another window
17.10. Determination of the C–C Bond Strength of Substituted Cyclopropanes and Cyclobutanes using Bomb Calorimetry p903-907 By Steffanie H. Liskey ; Steffanie H. Liskey Department of Chemistry, Virginia Tech 1040 Drillfield Drive, Blacksburg VA 24061 USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar Alan R. Esker ; Alan R. Esker Department of Chemistry, Virginia Tech 1040 Drillfield Drive, Blacksburg VA 24061 USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar J. M. Tanko J. M. Tanko Department of Chemistry, Virginia Tech 1040 Drillfield Drive, Blacksburg VA 24061 USA [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 17.10. Determination of the C–C Bond Strength of Substituted Cyclopropanes and Cyclobutanes using Bomb Calorimetry in another window
18.1. Resolution of a Chiral Amine and Recovery of Unwanted Enantiomer by Racemization: Towards a Greener Industrial Process p908-913 By Pedro P. Santos ; Pedro P. Santos CQE, Department of Chemical Engineering, IST, University of Lisbon Av. Rovisco Pais 1649-003 Lisbon Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Pedro F. Pinheiro Pedro F. Pinheiro CQE, Department of Chemical Engineering, IST, University of Lisbon Av. Rovisco Pais 1649-003 Lisbon Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 18.1. Resolution of a Chiral Amine and Recovery of Unwanted Enantiomer by Racemization: Towards a Greener Industrial Process in another window
18.2. Synthesis of Racemic Phenylalanine Methyl Ester and its Kinetic Resolution Catalysed by α-Chymotrypsin p914-918 By Luca Banfi ; Luca Banfi Department of Chemistry and Industrial Chemistry, University of Genova via Dodecaneso 31 16146 Genova Italy [email protected] Search for other works by this author on: This Site PubMed Google Scholar Renata Riva Renata Riva Department of Chemistry and Industrial Chemistry, University of Genova via Dodecaneso 31 16146 Genova Italy [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 18.2. Synthesis of Racemic Phenylalanine Methyl Ester and its Kinetic Resolution Catalysed by α-Chymotrypsin in another window
18.3. Lipase Catalyzed Kinetic Resolution of Racemic 1-Phenylethanol p919-922 By Otto Långvik ; Otto Långvik Johan Gadolin Process Chemistry Centre, Laboratory of Organic Chemistry, Åbo Akademi University Piispankatu 8 FI-20500 Turku Finland [email protected] Search for other works by this author on: This Site PubMed Google Scholar Tiina Saloranta ; Tiina Saloranta Johan Gadolin Process Chemistry Centre, Laboratory of Organic Chemistry, Åbo Akademi University Piispankatu 8 FI-20500 Turku Finland [email protected] Search for other works by this author on: This Site PubMed Google Scholar Reko Leino Reko Leino Johan Gadolin Process Chemistry Centre, Laboratory of Organic Chemistry, Åbo Akademi University Piispankatu 8 FI-20500 Turku Finland [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 18.3. Lipase Catalyzed Kinetic Resolution of Racemic 1-Phenylethanol in another window
18.4 Enzymatic Kinetic Resolution and Separation of sec -Alcohols Methodology Based on Fatty Esters p923-926 By Carlos M. Monteiro ; Carlos M. Monteiro iMed. ULisboa, Faculdade de Farmácia da Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Nuno M. T. Lourenço ; Nuno M. T. Lourenço Department of Bioengineering, IBB – Institute for Biotechnology and Bioengineering, Centre for Biological and Chemical Engineering, Instituto Superior Técnico 1049-001 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso iMed. ULisboa, Faculdade de Farmácia da Universidade de Lisboa Av. Prof. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 18.4 Enzymatic Kinetic Resolution and Separation of sec-Alcohols Methodology Based on Fatty Esters in another window
18.5. Enzymatic Kinetic Resolution and Preparative Separation of Secondary Alcohols p927-930 By Nuno M. T. Lourenço ; Nuno M. T. Lourenço Instituto Superior Técnico, Universidade de Lisboa Av. Rovisco Pais, 1 1049-001 Lisboa Portugal [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos M. Monteiro ; Carlos M. Monteiro Faculdade de Farmácia, Universidade de Lisboa Av. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Carlos A. M. Afonso Carlos A. M. Afonso Faculdade de Farmácia, Universidade de Lisboa Av. Gama Pinto 1649-003 Lisboa Portugal [email protected] [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 18.5. Enzymatic Kinetic Resolution and Preparative Separation of Secondary Alcohols in another window
18.6. Catalyzed Resolution and Simultaneous Selective Crystallization p931-934 By Jaan Parve ; Jaan Parve Institute of Technology, University of Tartu Nooruse 1 50411 Tartu Estonia Search for other works by this author on: This Site PubMed Google Scholar Lauri Vares ; Lauri Vares Institute of Technology, University of Tartu Nooruse 1 50411 Tartu Estonia Search for other works by this author on: This Site PubMed Google Scholar Indrek Reile ; Indrek Reile National Institute of Chemical Physics and Biophysics Akadeemia tee 23 12618 Tallinn Estonia Search for other works by this author on: This Site PubMed Google Scholar Tõnis Pehk ; Tõnis Pehk National Institute of Chemical Physics and Biophysics Akadeemia tee 23 12618 Tallinn Estonia Search for other works by this author on: This Site PubMed Google Scholar Ly Villo ; Ly Villo Department of Chemistry, Tallinn University of Technology Ehitajate tee 5 19086 Tallinn Estonia [email protected] Search for other works by this author on: This Site PubMed Google Scholar Omar Parve Omar Parve Department of Chemistry, Tallinn University of Technology Ehitajate tee 5 19086 Tallinn Estonia [email protected] Search for other works by this author on: This Site PubMed Google Scholar Open the PDF Link PDF for 18.6. Catalyzed Resolution and Simultaneous Selective Crystallization in another window
Subject Index p935-951 Open the PDF Link PDF for Subject Index in another window

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James M. Postma

Dr. James Postma is a physical chemist at California State University, Chico.  He received his Ph.D. from UC Davis in 1982, studying electrochemistry with Dr. Peter Rock to evaluate the Born-Oppenheimer Approximation.  He joined the faculty at CSU, Chico in 1982 and teaches courses in physical and analytical chemistry as well as general chemistry courses.  He is the co-author of General Chemistry in the Laboratory, 7th edition , a widely-used laboratory textbook in freshman chemistry classes.  He is the chair-elect of the California Section of the American Chemical Society and is currently the Chair of the Academic Senate of the California State University system.  He has been a member of the California Science Project Advisory Board since 1995 and has chaired the Board since 2000.

Anne Roberts

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Expertly communicate the excitement of chemistry with these time-tested classroom practicals.

These resources have been compiled from the book Classic chemistry experiments : a collection of 100 chemistry experiments developed with the support of teachers throughout the UK.

If you'd like to buy a copy of the book, visit our online bookshop . If you're a Royal Society of Chemistry member, don't forget to use your 35% discount.

A Cartesian diver

An old favourite experiment, the Cartesian diver is easy for students to complete. Explore important ideas that build a foundation of knowledge.

Chemistry and electricity

Create coloured writing from acids, alkali, and salt solution, all activated through electrolysis.

Disappearing ink

Explore the reaction between acids and bases as students create disappearing ink, in this favourite classroom practical.

Electricity from chemicals

Use various metals, in pairs, and n electrolyte to form a cell. Then observe the formation of ions around the reactive metal, and compare the speed with which they form around the less reactive metal. Includes kit list and safety instructions.

Experiments with particles

Explore physical states, and how material interact with three practicals. Students use common classroom items to explore, and then note their findings. Includes kit list and safety instructions.

Three small candles or tea lights burning against a black background

Identifying the products of combustion

In association with Nuffield Foundation

Illustrate the presence of water and carbon dioxide in the products of hydrocarbon combustion in this demonstration. Includes kit list and safety instructions.

Particles in motion?

Explore the movement of gas particles in this practical but reacting calcium carbonate with hydrochloric acid. Includes kit list and safety instructions.

Producing a foam

Explore foams and their properties in this experiment, so students learn how foam is produced and produce their own. Includes kit list and safety instructions.

Properties of the transition metals and their compounds

Student discover the diversity of transition metals in this practical that puts their knowledge of these common elements to the test. Includes kit list and safety instructions.

Rubber band experiment

A rubber band, a hairdryer, and a curious mind will see students discover the principles of heat based reactions. Includes kit list and safety instruction.

Testing salts for anions and cations

A full range of chemicals will guide students into discovering how to identify the composition of unknown substances. Includes kit list and safry instructions.

The effect of concentration and temperature on reaction rate

Reaction rate can be altered by many things, in this practical students explore how temperature and concentration effect reaction in an closer look at kinetics. Includes kit list and safety instructions.

The effect of temperature on reaction rate

Discover more about collision theory in this practical, where a sodium thiosulfate and hydrochloric acid mixture produce an interesting reaction. Includes kit list and safety instructions.

The effect of temperature on solubility

Hot or cold, which water is better for soluble substances? Explore your finding from this practical into the effect of temperature on solubility. Includes kit list and safety instructions.

The electrolysis of solutions

Electricity is passed through various solutions and the products are identified. Includes kit list and safety instructions

The preparation and properties of oxygen

Produce a potassium manganate(VII) reaction using a test tube, Bunsen burner, and scientific inquisition to detect the presence of oxygen. Includes kit list and safety instructions.

The reactivity of the group 2 metals

Compare group 1 and group 2 metals with this practical that shows their reactivity rates, where students can take control of their own observations and come to their own conclusions

The volume of 1 mole of hydrogen gas

Understand the volume of one mole of hydrogen gas through a magnesium and acid reaction, taking note of the temperature and pressure. Includes kit list and safety instructions.

Compare the viscosity of thick and thin liquids in this experiment, which gets young learners exploring how viscosity alters the speed of an air bubble through the substances. Includes kit list and safety instructions.

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Experimental Physical Chemistry: A Laboratory Textbook

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Experimental Physical Chemistry: A Laboratory Textbook Third Edition

ISBN-10 0716717352
ISBN-13 978-0716717355
Edition Third
Publisher W. H. Freeman
Publication date June 30, 2006
Language English
Dimensions 8.75 x 1.26 x 11.22 inches
Print length 608 pages
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Product details

Publisher ‏ : ‎ W. H. Freeman; Third edition (June 30, 2006)
Language ‏ : ‎ English
Hardcover ‏ : ‎ 608 pages
ISBN-10 ‏ : ‎ 0716717352
ISBN-13 ‏ : ‎ 978-0716717355
Item Weight ‏ : ‎ 3.15 pounds
Dimensions ‏ : ‎ 8.75 x 1.26 x 11.22 inches
#152 in Physical Chemistry
#1,557 in Chemistry (Books)
#1,987 in General Chemistry

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Arthur m. halpern.

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Yuzhno-Sakhalinsk city, Russia

The capital city of Sakhalin oblast .

Yuzhno-Sakhalinsk - Overview

Yuzhno-Sakhalinsk is a city located in the southern part of Sakhalin Island in the Far East of Russia, the administrative center of Sakhalin Oblast.

The population of Yuzhno-Sakhalinsk is about 201,700 (2022), the area - 164 sq. km.

The phone code - +7 4242, the postal codes - 693000-693904.

Yuzhno-Sakhalinsk city flag

Yuzhno-sakhalinsk city coat of arms.

Yuzhno-Sakhalinsk city map, Russia

Yuzhno-sakhalinsk city latest news and posts from our blog:.

29 October, 2019 / Yuzhno-Sakhalinsk - the view from above .

History of Yuzhno-Sakhalinsk

Foundation of yuzhno-sakhalinsk.

The Russians first visited Sakhalin Island in 1742. In 1805, the Russian-American Company sent Adam Johann von Krusenstern, a Russian admiral and explorer, to Sakhalin to hoist the Russian flag on the island. Officially, neither Russia nor Japan claimed Sakhalin and the Kuril Islands. In 1855, a treatise on friendship and the border was signed in Shimoda, which marked the beginning of diplomatic relations between Russia and Japan. According to it, Sakhalin remained jointly owned by the two countries.

The settlement of Sakhalin by Russians was mainly due to exiled convicts. In 1869, Sakhalin was officially declared a place of exile and hard labor. In 1875, the St. Petersburg Treaty was signed between the Russian Empire and Japan, according to which Sakhalin completely went to Russia and the Kuril Islands - to Japan.

In 1881, according to the order of the military governor of the Primorsky region, Major Vladimir Yantsevich was appointed head of exiles in South Sakhalin. He received the following instructions: “For the settlement of those who are finishing their terms of hard labor, a place that is quite convenient for arable farming should be chosen. The selected site, if possible along the main road from south to north, should be planned, divided into sections and, as a new settlement, named by some permanent name.”

In 1883, Yantsevich applied for the approval of the names of four new villages founded in the south of Sakhalin: Solovyovskoe, Mitsulskoe, Vladimirovka (future Yuzhno-Sakhalinsk), and Vlasovskoe. In 1885, 57 people lived in Vladimirovka, in 1895 - 130 people. In 1897, there were 150 residential and commercial buildings here: a church, a school, a post office, a hospital, a mill, trade shops, a number of government buildings, and a lot of residential log houses.

More historical facts…

Japanese period in the history of Yuzhno-Sakhalinsk

In 1905, after the defeat of the Russian Empire in the Russo-Japanese War, according to the Treaty of Portsmouth, part of Sakhalin south of the 50th parallel was ceded to the Japanese Empire and became the Karafuto Prefecture. The northern part of Sakhalin remained under the control of the Russian Empire.

In 1908, Vladimirovka was renamed Toyohara (“bountiful plain”). In 1915, the settlement received the status of a town. The Japanese made their own plan for the development of the town with a clear rectangular planning system with the direction of streets along the railway and perpendicular to it.

The building density was high, as a result, a significant number of residential buildings were without outbuildings, sheds and other ancillary buildings, as well as yards. On the outskirts of the town there was a well-maintained park with an artificial reservoir. In 1920, the population of Toyohara was 14,176 people, in 1935 - 28,459.

On February 11, 1945, Stalin, Roosevelt and Churchill signed an agreement in Yalta on the conditions for the USSR’s entry into the war against Japan. Among the conditions were the return of South Sakhalin to the USSR and the annexation of the Kuril Islands. In August 1945, Soviet troops entered Toyohara.

This is what Toyohara looked like from the words of Dmitry Kryukov, head of the civil administration of South Sakhalin and the Kuril Islands, who arrived in the town in September 1945: “The town mainly consists of wooden buildings. The houses are adjacent to each other, timber-frame, plastered. Many of them look good, but they are cold.” The majority of the population were Japanese and Koreans.

Yuzhno-Sakhalinsk - the capital of Sakhalin Oblast

On February 2, 1946, Yuzhno-Sakhalin Oblast was formed on the territory of South Sakhalin and the Kuril Islands. On June 4, 1946, Toyohara became its administrative center. It was renamed Yuzhno-Sakhalinsk (“South Sakhalin City”).

On January 2, 1947, Yuzhno-Sakhalin Oblast was liquidated and its territory was included in Sakhalin Oblast, a separate region of the Russian Soviet Federative Socialist Republic. On April 18, 1947, Yuzhno-Sakhalinsk became its administrative center.

In the spring of 1947, the mass repatriation of the Japanese began. By August 1, 1947, 124,308 people left Sakhalin, almost half of the local Japanese. During 1947-1949, about 400 thousand people were brought to Sakhalin from the central regions of Russia, Primorye and the Far East. By 1949, only 2,682 Japanese remained on Sakhalin - those who managed to obtain a Soviet passport. The Koreans from Sakhalin were not forcibly evicted, so most of them stayed. In 1959, the population of Yuzhno-Sakhalinsk was 85,510 people.

In subsequent years, the appearance of Yuzhno-Sakhalinsk changed again - the frame houses built by the Japanese were demolished. Today, except for the railway and some buildings of that time turned into museums, almost nothing reminds of the Japanese period in the history of this city.

General views of Yuzhno-Sakhalinsk

Yuzhno-Sakhalinsk from above

Author: Vladislav Yarowind

General view of Yuzhno-Sakhalinsk

Yuzhno-Sakhalinsk cityscape

Author: Shinya Ichinohe

Yuzhno-Sakhalinsk - Features

Sakhalin Oblast is the only region in Russia located entirely on the islands. Yuzhno-Sakhalinsk stands at some distance from the sea coast, about 25 km from the coast of the Sea of Okhotsk. Chekhov Peak (1,045 m), one of the highest peaks of Sakhalin, rises to the north-east of the city. Locals call the city simply Yuzhnyy.

Sakhalin Island is part of the temperate monsoon zone. Yuzhno-Sakhalinsk is located on a plain surrounded by hills, due to which its climate has certain peculiarities. In summer, it can be very hot in Yuzhno-Sakhalinsk, and in winter, due to the lack of wind, severe frosts. The coldest month is January with an average daily temperature of minus 12.2 degrees Celsius, the warmest month is August with an average daily temperature of plus 17.3 degrees Celsius. Yuzhno-Sakhalinsk is equated to the regions of the Far North.

The city is located in an earthquake-prone area. The probability of strong earthquakes is relatively high. The distance from Yuzhno-Sakhalinsk to Moscow is 9,140 km by road and 6,640 km in a straight line.

The majority of the population is Russian, but the proportion of Koreans is also high (about 20%). Out of 43 thousand Sakhalin Koreans, most of them live in the capital of the region. In the city you can also find representatives of the indigenous peoples: Nivkhs, Ainu and Oroks, but their number is very small.

Yuzhno-Sakhalinsk is the largest transport hub on Sakhalin. Anton Chekhov Yuzhno-Sakhalinsk Airport offers regular flights to such cities as Vladivostok, Krasnoyarsk, Novosibirsk, Khabarovsk, Moscow, Komsomolsk-on-Amur, Petropavlovsk-Kamchatsky, Seoul (South Korea), Sapporo (Japan), Tokyo (Japan).

In Yuzhno-Sakhalinsk, there is a high level of air pollution due to the high motorization of the population and the location of the city in the valley, which slows down the dispersion of harmful substances.

Today, it is one of the dynamically developing cities of the Far East, the production and intellectual center of Sakhalin and the Kuril Islands. Oil and natural gas production, as well as their processing, are the most important components of the local economy.

This is one of the most visited cities in the Far Eastern Federal District of Russia. Yuzhno-Sakhalinsk is often visited by cruise ship passengers (mostly Japanese citizens). Restaurants of Yuzhno-Sakhalinsk offer dishes of Russian, Chinese, Korean, Japanese, Uzbek, Georgian, Italian cuisines.

The architecture of the period of the Karafuto Prefecture gives a special flavor to Yuzhno-Sakhalinsk. Today, in the city there are about 40 objects of cultural heritage of this period. In the future, tourism should become the basis for the economic development of Yuzhno-Sakhalinsk.

Special thanks to Vladislav Yarowind for the photos of Yuzhno-Sakhalinsk.

Main Attractions of Yuzhno-Sakhalinsk

Sakhalin Regional Museum of Local Lore - the central museum of Sakhalin Oblast founded in 1896. It is housed in a very picturesque Japanese building constructed in the Imperial Crown Style in 1937. This is the only such building on the territory of Sakhalin and all of Russia, the most significant architectural monument of Yuzhno-Sakhalinsk. Its diverse expositions are devoted to nature, history of the indigenous peoples of the islands, culture and development of Sakhalin. Kommunisticheskiy Avenue, 29.

Sports and Tourist Complex “Gornyy Vozdukh” (“Mountain Air”) - a ski resort and sports complex, existing, according to one version, since the days of the Japanese Karafuto Prefecture (1905-1945). Today, it is one of the most dynamically developing ski resorts in the Far East of Russia.

The unique location of the complex - in the center of Yuzhno-Sakhalinsk - allows guests to find themselves in the world of winter sports in just a few minutes. The ski resort offers 10 slopes of various difficulty levels for both beginners and professionals. Their total length is over 23 km. The ski season lasts from December to the end of April.

It is one of the main organizers of excursion tours in Sakhalin Oblast: sports, excursion, business tourism, as well as ecological tourism. The complex has a network of hiking and cycling routes. There are also restaurants and cafes here.

Museum and Memorial Complex “Pobeda” (“Victory”) - a square with a cultural and educational center, where you can find historical expositions dedicated to the Russian-Japanese and World War II. A T-34-85 tank is installed on a pedestal in front of the building. Pobedy Avenue, 1.

Museum of the History of the Sakhalin Railway . This museum is dedicated to the history of railway construction on Sakhalin. The exposition has a lot of interesting and rare exhibits. In the open area of the museum, Sakhalin railway equipment is exhibited: steam locomotives, carriages of various types, etc. Vokzalnaya Street, 55.

Sakhalin Regional State Art Museum - the only art museum in Sakhalin Oblast with over 11 thousand works of art. On the ground floor, temporary art exhibitions are held, the art of artists from Russia, Korea and China is presented. The second floor houses permanent exhibitions: “Contemporary Korean Art”, “Christian Art”, “Russian Art of the 19th - early 20th centuries.” Lenina Street, 137.

Museum of the Book of Anton Chekhov “Sakhalin Island” . This museum is dedicated to Anton Chekhov’s trip to Sakhalin in 1890, as a result of which he wrote the book “Sakhalin Island”. Here you can find the following collections: “Painting”, “Graphics”, “Written Sources”, “Photo Materials”, “Numismatics/Phaleristics”, “Household Items, Arts and Crafts”, “Sculpture”. The personal belongings of Chekhov’s family members and various items belonging to exiles are exhibited here. Mira Avenue, 104.

Yuzhno-Sakhalinsk Park of Culture and Rest named after Yuri Gagarin - the most beautiful recreational area of Yuzhno-Sakhalinsk founded in the Japanese period of the city’s history in 1906. In 1968, when the famous cosmonaut Yuri Gagarin died in a jet crash, the park was renamed in his honor. Today, this place attracts visitors with its amazing landscapes and an abundance of entertainment. Sakura blooms here in spring. Detskaya Street, 1.

Resurrection Cathedral - the first church in Yuzhno-Sakhalinsk built in the 1990s. This one-domed cathedral in the pseudo-Russian style looks surprisingly graceful and is located in the immediate vicinity of Gagarin Park. Svyatitelya Innokentiya Boulevard, 3k1.

Cathedral of the Nativity . The height of this church, consecrated in 2016, is 77 m, which is why it effectively dominates the surrounding landscape. Accommodating up to 1,000 people, it is built in the Novgorod style with a gilded dome surrounded by four bright blue ones. Inside, you can admire the five-tiered iconostasis in the Russian style, decorated with 98 icons. The outer walls are decorated with mosaics created in Jerusalem. Ilarion Troitsky Street, 1.

Chekhov Peak . Several picturesque mountain peaks are located in the vicinity of Yuzhno-Sakhalinsk. The highest one (1,045 m) is named after the famous Russian writer Anton Chekhov. The trip to the top takes several hours. From the height of Chekhov Peak you can admire the city itself, the waters of Aniva Bay and the Sea of Okhotsk. On a cloudless day, you can even see the northern tip of the Japanese island of Hokkaido. There is a small Japanese temple at the top of the peak.

Yuzhno-Sakhalinsk city of Russia photos

Architecture of yuzhno-sakhalinsk.

Winter in Yuzhno-Sakhalinsk

Yuzhno-Sakhalinsk architecture

Yuzhno-Sakhalinsk modern architecture

Author: Alexander Mikhalev

Churches of Yuzhno-Sakhalinsk

Wooden Church of St. Nicholas in Yuzhno-Sakhalinsk

The Roman Catholic Church Parish of Saint James in Yuzhno-Sakhalinsk

Resurrection Cathedral in Yuzhno-Sakhalinsk

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Harris Chooses Walz

A guide to the career, politics and sudden stardom of gov. tim walz of minnesota, now vice president kamala harris’s running mate..

This transcript was created using speech recognition software. While it has been reviewed by human transcribers, it may contain errors. Please review the episode audio before quoting from this transcript and email [email protected] with any questions.

Hey, it’s Michael. Before we get started, I want to tell you about another show made by “The New York Times” that pairs perfectly with “The Daily.” It’s called “The Headlines.” It’s a show hosted by my colleague, Tracy Mumford, that quickly catches you up on the day’s top stories and features insights from “The Times” reporters who are covering them, all in about 10 minutes or less.

So if you like “The Daily”— and if you’re listening, I have to assume you do — I hope that means you’re going to “The Headlines” as well. You can now find “The Headlines” wherever you get your podcasts. So find it, subscribe to it, and thank you. And now, here’s today’s “Daily.”

From “The New York Times,” I’m Michael Barbaro. This is “The Daily.”

[MUSIC PLAYING]

Today, the story of how a little known Midwestern governor became Kamala Harris’s choice for a running mate. My colleague Ernesto Londoño walks us through the career, politics, and sudden stardom of Governor Tim Walz of Minnesota.

It’s Wednesday, August 7.

Ernesto, over the past few days, we watched Vice President Harris bring the final three contenders for her running mate to her house in Washington, DC, for a set of in-person interviews. And then we watched as she seemed to narrow her pool of choices down to a final two — the governor of Pennsylvania, Josh Shapiro, and the governor of Minnesota, Tim Walz. And now, of course, we know that she has made her choice. What has she told us about her campaign strategy, the way she views this race, in ultimately choosing Tim Walz?

Michael, I think what the choice tells us is that Kamala Harris was drawn to two qualities that Governor Walz brings to the table. And what’s interesting is they may seem to be in tension. For starters, here’s the ultimate everyday man, somebody who grew up in a small town in Middle America, served in the National Guard, was a high school teacher, a football coach, very plain-spoken, goes to campaign events wearing T-shirts and baseball caps, is a gun owner and very proud about it. He sort of embodies the Midwest.

And she clearly thinks that that is going to bring the kind of moderate, white, working class voters that the campaign needs in swing states to come to them, to make this feel like a balanced ticket and something that will give her enough of the crucial votes to defeat Donald Trump in the fall.

On the other hand, as governor, he passed a slew of pretty progressive legislation in the past couple of years, everything from abortion rights to gun control. So these things are likely to appeal to bread and butter Democrats.

But the question is, when voters have examined these two facets of Tim Walz, may it bring them enough enthusiasm from the base and enough undecided voters that the campaign desperately needs, or at some point, do these two aspects of him start canceling each other out?

Right. In short, you’re saying Harris is betting on a dual appeal from Walz to two essential constituencies, but the risk is that the appeal to one of them is just much, much greater than to the other.

Right. You could definitely see a scenario where voters, once they’ve examined Tim Walz’s story and legacy, may conclude that both of these candidates are quite liberal.

OK, so tell us the story of Tim Walz, a story that I think a lot of us don’t know because we really don’t know Walz all that well, and how he has come to embody these two qualities and that tension that you just described.

Michael, the origin story of Tim Walz’s political career is quite fascinating.

He and his wife were teachers in a small city south of Minneapolis. And in 2004, when George W. Bush was running for re-election, Walz took a group of his students to a political rally in his hometown. They wanted to just see the president make his case. And a strange scuffle happened when they were trying to get in.

Well, one of the kids had a John Kerry sticker on his wallet. And this is where the individual says, well, you’re not going to be allowed to enter. You’ve been deemed a threat.

Apparently, one of the students had a sticker for Bush’s rival, John Kerry, on his wallet. And security officials at the rally didn’t want to let them in.

And I said, oh, it’s OK. They’re with me. And who are you? And I said, I’m Tim Walz. I’m their teacher here, and showed them my ID. And they said, well, you two have been deemed a threat to the president. And I said, well, that’s not true. And it kind of escalated.

And this really ticked off Tim Walz. He was really upset. There was a fight and a confrontation at the rally.

At this point in time, I’m kind of nervous. I’m getting arrested. So I’m like saying, well, I’m Teacher of the Year in Mankato. And they didn’t care about that. And it was kind of a sad epiphany moment, how it felt for people to be looked right through by people. These people didn’t see me. And this is happening.

And ultimately, he sort of walks away from this moment feeling really sick of the Bush administration, the politics of the day. And he turns around and volunteers for the Kerry campaign.

And then the more interested he becomes in politics in this era, he starts looking around his congressional district, and there’s a Republican who’s held the seat for many, many years. This was a largely rural district in southern Minnesota. And there’s no reason to believe that a newcomer to politics, somebody without a donor base, could make a run for this seat and win.

But Walz signs up for this weekend boot camp, where expert campaigners train newcomers who want to run for office. And he gets really enthused by the idea that he can pull it off. So he starts raising money with the support of an army of students who become so thrilled and energized by the prospect that their nerdy and kind geography teacher is making this uphill bid for a congressional race.

So his campaign staff is basically his former students.

That’s right. And he proves to be a formidable candidate. He draws a lot of attention to his experience in the classroom and as a coach.

When I coached football, these stands held about 3,000 people. That’s a lot. It’s also the number of American soldiers who have died fighting in Iraq.

He’s a very strong advocate for pulling out of the war in Iraq.

Serving right now are kids that I taught, coached, and trained to be soldiers. They deserve a plan for Iraq to govern itself, so they can come home.

And one thing that happens in the campaign that is really surprising to people is he comes out as being in favor of same-sex marriage. Now, it’s useful to remember that this is 2006, when the vast majority of Democrats, Democrats running for most elected office, were not ready to come out in favor of same-sex marriage.

And here’s a guy who’s new to politics, who’s trying to unseat a Republican who’s held on to his seat for more than 12 years, taking what appeared to be a reckless position on something. And when he was asked about it at the time, Tim Walz told a supporter, this just happens to be what I believe in. And I’d rather lose a race that I’ve ran being true and consistent to my values than try to run as somebody I’m not.

And of course, he wins.

Yes. To everybody’s surprise, he pulled it off.

So from the get-go, he shows a kind of maverick, “politics be damned” quality, taking stands that he knows may be unpopular among the voters he’s trying to win over. But he’s got some innate political gifts that are all making it work.

Yeah, I think that first campaign showed us that Tim Walz had real political chops. He was a very effective campaigner. And people really liked him. When he was knocking on doors, when he was introducing himself to voters, they saw him as somebody who was very genuine and who was admirable.

So once he gets elected in this conservative leaning district in Minnesota, what does he actually do in Congress?

In Congress, he develops a reputation for being somebody who can work across the aisle. And this is a period where Democrats and Republicans were deeply polarized over the Iraq War. He spends a lot of his time lobbying to expand benefits for veterans, so it’s easier for them to go to college after their service, and also becomes a leading voice in the quest to repeal Don’t Ask, Don’t Tell, the policy that prohibited openly gay servicemen from serving in uniform.

And he remained really popular. He easily won re-election five times. The last time he runs for his seat happens to be 2016, when President Trump wins his district by about 15 points.

And still, voters kept Tim Walz in office.

I think it’s important to note what you just said. Walz is distinguishing himself as a Democrat who can take some pretty progressive positions, as he did in that first campaign on gay rights, as he did with Don’t Ask, Don’t Tell, and keep winning in very Trump-friendly districts of his state.

That’s right. And as he’s serving his sixth term in office, he sets his sights on the governor’s mansion and decides to run for office in 2018. He wins that race easily. And early on, during his time as governor, the eyes of the world are on Minnesota after a police officer kills George Floyd. And what we see is massive looting and protests in Minneapolis.

Right, and remind us how Governor Walz handles that violence, those protests.

Yeah, I think that’s a crucial chapter in Tim Walz’s political career and one that will come under scrutiny in the days ahead.

After George Floyd was killed on a Monday —

People are upset, and they’re tired. And being Black in Minnesota already has a stigma and a mark on your back.

— protests took root in Minneapolis.

Y’all want to sit out here and shoot off your rubber bullets and tear gas.

And they got progressively larger and more violent.

There comes a point where the mayor and the police chief in Minneapolis plead for help. They ask the governor to send in the National Guard. And crucially, that request was not immediately heeded.

This is the third precinct here. There are fires burning to the left of it at the —

And at the height of the crisis, a police precinct building was abandoned.

There’s someone climbing up the wall right now, kicking the window in, trying to climb up the wall.

Because city officials grew concerned that protesters were about to overrun it and may attack the cops inside their own turf.

[EXPLOSIONS]

And the building is set on fire.

Right, a very memorable image. I can recall it happening in real-time.

Yeah, and in the days that followed, I think there were a lot of questions of why the governor didn’t send in troops earlier and whether a more muscular, decisive response could have averted some of the destruction that spread through the city.

And how does Walz end up explaining his decision not to send in the National Guard more quickly?

The governor and his administration have said that they were really, really dealing with an unprecedented challenge. And I think there was a concern that sending in troops into this really, really tense situation could have done more to escalate rather than pacify things on the street.

But in the weeks and months that followed, there were a lot of questions about Governor Walz’s leadership. And there were critics who said, during what may have been the most challenging week of his life, we saw a governor who was indecisive and who waited too long to send in resources that ultimately allowed the city to get to a semblance of order.

Right, and it feels like this is a moment that will almost assuredly be used against him by Donald Trump and JD Vance, the Republican ticket, which has made law and order so central to their message in this campaign.

Yeah, absolutely. And here in Minnesota, that was certainly a liability for him when he ran for re-election in 2022. But voters kept him in office, and he won that race handily. And not only did he win, but Democrats managed to flip the Senate and have full control of the legislature on his watch.

And that sets in motion one of the most productive legislative sessions in Minnesota history, where Tim Walz and his allies in the House and the Senate managed to pass a trove of really progressive legislation, oftentimes on a party vote.

Tell us about some of that legislation.

Well, Minnesota becomes the first state in the wake of the Supreme Court ending the constitutional right to abortion to actually codify this right under state statute. And they did a lot more stuff. They had a huge budget surplus, and they used that, for instance, to fund meals for all school children.

They managed to pass a couple of gun control laws that were very contentious. They gave the right to undocumented immigrants to get driver’s licenses. They legalized recreational marijuana. And finally, the governor takes a pretty bold stance on this issue of gender affirming care for transgender kids and teenagers, and says that Minnesota will be a safe haven for people who want that health care.

So, Ernesto, so how should we think about that blitz of legislation and the largely progressive tone of it, given the way that Walz had campaigned and succeeded up to that moment as somebody with such broad appeal across the political spectrum?

When the governor was asked whether this had been too much too quickly in terms of progressive legislation, his answer was that these were broadly popular policies, that these are issues Democrats had campaigned on. And here, Democrats had a window of opportunity where they were in control of the governor’s mansion and control of the House, the Senate, and that when you have political capital, you spend it.

But when you start listening to Republicans in Minnesota, they say, here’s a guy who campaigned on this mantra of “One Minnesota.” That was his campaign slogan. And he sort of came into office with this promise that he would govern in a bipartisan way, reach across the aisle.

But when they had all the votes they needed to pass their policies, Republicans felt that Walz was not bothering to bring them into the fold and to pass legislation that was going to be palatable to conservatives in the state. So I think people who once regarded him as a moderate now start seeing him as somebody who, when he had the power, acted in ways that were really progressive and liberal.

So at the height of his power, Governor Walz emerges as somebody who, when given a shot at getting done what he really wants to get done with a Democratic legislature, is a pretty progressive leader, even at the risk of being somewhat at odds with his earlier image as more moderate, because in his mind, enough people in the state are behind these policies.

Yeah, and I think he assumed that he had banked enough goodwill and that people across the state liked him enough to tolerate policies they may have disagreed with. And I think it’s safe to say, among the people who cover him here regularly, there was never any real hint that Tim Walz was eyeing a run for higher office. He’s not somebody who has written the kind of political memoir that oftentimes serves as a case of what you would bring to a national ticket or to the White House. And he seems pretty happy with a state job.

So it was a huge surprise when Tim Walz starts going viral through a string of cable news appearances right after President Biden drops out of the race, and the Democrats are scrambling to put Harris at the top of the ticket. And what becomes clear is that Walz is very forcefully auditioning for the role of vice president, and Vice President. Harris starts taking him very seriously.

We’ll be right back.

So, Ernesto, tell us about this cable news audition that Governor Walz undertakes over the past few weeks and how, ultimately, it seemed to help him land this job of being Harris’s running mate.

I think Walz does something really interesting, and that is that he says that Democrats shouldn’t be talking about Trump and Vance as existential threats. He kind of makes the case that Democrats have been in this state of fear and paralysis for too long, and that it’s not serving them well. So the word he latches onto is “weird.”

Well, it’s true. These guys are just weird.

It is. It is.

And they’re running for he-man women hater’s club or something. That’s what they go at. That’s not what people are interested in.

And I think one other thing we see in Walz is somebody who’s putting himself out there as a foil to JD Vance.

That angst that JD Vance talks about in “Hillbilly Elegy,” none of my hillbilly cousins went to Yale, and none of them went on to be venture capitalists or whatever. It’s not —

I think the case he’s making is that Tim Walz is a more authentic embodiment of small town values.

What I know is, is that people like JD Vance know nothing about small town America. My town had 400 people in it, 24 kids in my graduating class. 12 were cousins. And he gets it all wrong. It’s not about hate.

And behind the scenes, people from Tim Walz’s days on Capitol Hill start calling everybody they know in the Harris campaign and the Harris orbit and saying, here’s a guy who has executive experience as governor, but also somebody who has a really impressive record from his time on Capitol Hill and somebody who could be an asset in helping a Harris administration pass tough legislation. So you should take a hard look at this guy.

Which is, of course, exactly what Harris ends up doing. And I want to talk for a moment about how Harris announces Walz as her running mate on Tuesday morning. She did it in an Instagram message. And it felt like the way she did it very much embraced this idea that you raised earlier, Ernesto, that Walz contains these two appeals, one to the Democratic base, one to the white working class.

Harris specifically cites the work that Walz did with Republicans on infrastructure and then cites his work on gun control. She mentions that he was a football coach and the founder of the high school Gay Straight Alliance. She’s straddling these two versions of Walz.

But I want to linger on the idea for a moment of Walz’s vulnerabilities, because once he becomes Harris’s running mate, Harris and Walz are going to lose a fair amount of control over how they present him to the country, because he’s going to become the subject of very fierce attacks from the Republicans in this race. So talk about that for just a moment.

Yeah, I mean, it’s important to keep in mind that Governor Walz has never endured the scrutiny of a presidential race. So the questions he’s going to be asked and the way his record is going to be looked at is going to be different and sharper. I think the Harris campaign is billing him as, first and foremost, a fighter for the middle class. And I think that certainly will have some appeal.

But I think in coming days, there’s going to be a lot of attention drawn to parts of his record that may be unpopular with many voters. For instance, giving undocumented immigrants driver’s licenses, which Governor Walz championed. It’s likely to provide fodder for an attack ad.

The very dramatic footage of Minneapolis burning in 2020 is also something that I think people will be drawn to. And there’s going to be interest in reexamining what the governor did and what he could have done differently to avert the chaos.

And on Tuesday, we saw that the Trump campaign wasted no time in trying to define Tim Walz as soft on crime, permissive on immigration policy. And they also made clear they wanted to relitigate the era of George Floyd’s killing. And specifically, they want to try to tie him to the effort at the time to defund the police, which is a movement that Walz personally never endorsed.

So the Republican attack here will be pretty simple. Walz is liberal. Harris is liberal. So, in their efforts to speak to especially white working class and rural voters in swing states, the Trump campaign is going to say this is not the ticket for that group of voters. This is the ticket of burning police precincts and gun control. And of course, that may not be fair, but that’s very likely going to be the message over the next couple of months.

Right. I think there’s going to be effort to portray him as a radical liberal who has used his small town roots to put on this sort of veneer of being a moderate and a really sort of understanding and being part of the segments of the electorate that I think are critical in this election.

I want to speak for just a moment about the person Harris did not pick when she chose Walz because many Democrats had felt that Walz was a potentially too liberal seeming running mate for a candidate, Kamala Harris, who herself comes from a blue state and is caricatured by the Republicans as liberal herself.

And the person she didn’t choose was Governor Josh Shapiro of Pennsylvania, who was seen as having a huge appeal in that particular key swing state, but also presented risks of his own of alienating parts of the Democratic base with his well-documented support for Israel and his criticism of campus protesters. How should we think about the fact that, ultimately, Harris chose Walz over Shapiro?

Yeah, I think in the final stretch of this campaign to be the vice presidential pick, we started seeing a lot of acrimony in pockets of the Democratic base, drawing attention to the fact that Governor Shapiro could be divisive on Gaza, which has really sort of split the party in recent months.

So I think at the end of the day, they made a calculation that Tim Walz would be more of a unifying figure and would be somebody who would inspire and energize enough pockets of the electorate that they need, particularly in the Midwest, to make him the stronger and more exciting pick and somebody who wouldn’t force them to go back to defending and relitigating the Biden administration’s record on Israel and on the war in Gaza.

Right, and then, on Tuesday night, we got our first glimpse of Harris and Walz together on stage for the first time at a campaign rally. I’m curious, what struck you about their debut together.

Good evening, Philadelphia.

I think everybody was watching the opening scene of this rally to see what the chemistry between these two people was going to be like. And they both seemed giddy. They were literally, at times, bouncing with enthusiasm.

Since the day that I announced my candidacy, I set out to find a partner who can help build this brighter future.

So Pennsylvania, I’m here today because I found such a leader.

Governor Tim Walz of the great state of Minnesota.

They soon got down to business. And that business was how to define Tim Waltz for voters who don’t know him well.

To those who know him best, Tim is more than a governor.

And right off the bat, we saw that Kamala Harris really highlighted a lot of pieces of his pre-political career.

To his former high school football players, he was Coach.

She repeatedly called him Coach Walz, Mr. Walz, evoking his time in the classroom, and even used his military title from his days in the Army.

To his fellow veterans, he is Sergeant Major Walz.

And then when it came time for Tim Walz to introduce himself on this massive stage —

Welcome the next vice president of the United States, Tim Walz.

— he drew a lot of attention to his small town roots.

I was born in West Point, Nebraska. I lived in Butte, a small town of 400.

He said something that he said repeatedly recently in campaign appearances, which is —

In Minnesota, we respect our neighbors and their personal choices that they make. Even if we wouldn’t make the same choice for ourselves, there’s a golden rule — mind your own damn business.

The golden rule of small towns is you mind your own damn business, which is something he said in the context of his argument that Republicans have been limiting, rather than expanding, people’s rights. But he also drew attention to the fact that he’s a gun owner.

By the way, as you heard, I was one of the best shots in Congress. But in Minnesota, we believe in the Second Amendment, but we also believe in common sense gun violence laws.

And then when it came time to draw a sharp contrast with their opponents, Tim Walz said, these guys are phonies.

Donald Trump is not fighting for you or your family. He never sat at that kitchen table like the one I grew up at, wondering how we were going to pay the bills. He sat at his country club in Mar-a-Lago, wondering how he can cut taxes for his rich friends.

He said it’s actually people like me and Kamala Harris who come from humble origins and showed what is possible in America when you hail from a working class background, and you seize opportunities that were available to you.

Thank you, Philadelphia. Thank you, Vice President. God bless America.

So when it comes to this question of Walz’s dual identities and dual appeals, what did we learn on day one of this new Democratic ticket, do you think?

I think the campaign is trying to convey that these two facets of Tim Walz’s life are not mutually exclusive, that they don’t need to be in tension. They don’t cancel each other out. They’re both part of Tim Walz’s story. And I think that’s how they’re going to present him from now until Election Day.

Ernesto, thank you very much. We appreciate it.

It’s my pleasure, Michael.

Here’s what else you need to know today. On Tuesday, Hamas said that Yahya Sinwar, one of the masterminds behind the deadly October 7 attacks on Israel, had consolidated his power over the entire organization. Until now, Sinwar had held the title of Hamas’s leader in Gaza. But with the assassination of Hamas’s top political leader by Israel last week, Hamas said that Sinwar would take on that title as well. Sinwar remains a major target of Israel and is believed to have been hiding in tunnels underneath Gaza since October 7.

And the US Department of Justice has charged a Pakistani man with ties to Iran with trying to hire a hitman to assassinate political figures in the United States. The man recently traveled to the US and was arrested in New York last month. American authorities believe that his potential targets likely included former President Trump.

Today’s episode was produced by Alex Stern, Eric Krupke, and Olivia Natt. It was edited by Lisa Chow and Patricia Willens, contains original music by Pat McCusker and Marion Lozano, and was engineered by Alyssa Moxley. Our theme music is by Jim Brunberg and Ben Landsverk of Wonderly. Special thanks to Nick Pittman and Minnesota Public Radio.

That’s it for “The Daily.” I’m Michael Barbaro. See you tomorrow.

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Hosted by Michael Barbaro

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Produced by Alex Stern Eric Krupke and Olivia Natt

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Earlier this summer, few Democrats could have identified Gov. Tim Walz of Minnesota.

But, in a matter of weeks, Mr. Walz has garnered an enthusiastic following in his party, particularly among the liberals who cheer on his progressive policies. On Tuesday, Vice President Kamala Harris named him as her running mate. Ernesto Londoño, who reports for The Times from Minnesota, walks us through Mr. Walz’s career, politics and sudden stardom.

On today’s episode

Ernesto Londoño , a reporter for The Times based in Minnesota, covering news in the Midwest.

Kamala Harris and Tim Walz waving onstage in front of a “Harris Walz” sign.

Background reading

Who is Tim Walz , Kamala Harris’s running mate?

Mr. Walz has faced criticism for his response to the George Floyd protests.

There are a lot of ways to listen to The Daily. Here’s how.

We aim to make transcripts available the next workday after an episode’s publication. You can find them at the top of the page.

The Daily is made by Rachel Quester, Lynsea Garrison, Clare Toeniskoetter, Paige Cowett, Michael Simon Johnson, Brad Fisher, Chris Wood, Jessica Cheung, Stella Tan, Alexandra Leigh Young, Lisa Chow, Eric Krupke, Marc Georges, Luke Vander Ploeg, M.J. Davis Lin, Dan Powell, Sydney Harper, Michael Benoist, Liz O. Baylen, Asthaa Chaturvedi, Rachelle Bonja, Diana Nguyen, Marion Lozano, Corey Schreppel, Rob Szypko, Elisheba Ittoop, Mooj Zadie, Patricia Willens, Rowan Niemisto, Jody Becker, Rikki Novetsky, Nina Feldman, Will Reid, Carlos Prieto, Ben Calhoun, Susan Lee, Lexie Diao, Mary Wilson, Alex Stern, Sophia Lanman, Shannon Lin, Diane Wong, Devon Taylor, Alyssa Moxley, Olivia Natt, Daniel Ramirez and Brendan Klinkenberg.

Our theme music is by Jim Brunberg and Ben Landsverk of Wonderly. Special thanks to Sam Dolnick, Paula Szuchman, Lisa Tobin, Larissa Anderson, Julia Simon, Sofia Milan, Mahima Chablani, Elizabeth Davis-Moorer, Jeffrey Miranda, Maddy Masiello, Isabella Anderson, Nina Lassam and Nick Pitman.

An earlier version of this episode misstated the subject that Walz’s wife taught. She taught English, not Social Studies.

How we handle corrections

Ernesto Londoño is a Times reporter based in Minnesota, covering news in the Midwest and drug use and counternarcotics policy. More about Ernesto Londoño

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Yuzhno-Sakhalinsk
Yuzhno-Sakhalinsk began as a small Russian settlement called Vladimirovka, founded by convicts in 1882. [2] The Treaty of Portsmouth in 1905, which brought an end to the Russo-Japanese War of 1904-1905, awarded the southern half of the Sakhalin Island to Japan.Vladimirovka was renamed Toyohara (meaning "bountiful plain"), and was the prefect capital of the Japanese Karafuto Prefecture.
Experimental Physical Chemistry: A Laboratory Textbook
This laboratory textbook is well-written. There are also supporting documents available from the book website. These documents lay out the materials and supplies needed and experimental precautions for each of the discussed experiments. There is also an excel program available for helping the experimenter to analyze the experimental data.
Yuzhno-Sakhalinsk
The climate in Yuzhno-Sakhalinsk is quite mild, there are no severe frosts in winter, and heat in summer. The coldest month is January with an average temperature of about minus 12 degrees Celsius. The warmest month is August (plus 17 degrees Celsius). Clear and dry weather sets in early September - the best time to visit Sakhalin.
Yuzhno-Sakhalinsk city, Russia travel guide
Yuzhno-Sakhalinsk - Overview. Yuzhno-Sakhalinsk is a city located in the southern part of Sakhalin Island in the Far East of Russia, the administrative center of Sakhalin Oblast. The population of Yuzhno-Sakhalinsk is about 201,700 (2022), the area - 164 sq. km. The phone code - +7 4242, the postal codes - 693000-693904.
Yuzhno-Sakhalinsk Map
Yuzhno-Sakhalinsk, also spelled Uzno-Sakhalinsk and previously known in Japanese as Toyohara, is the largest city and capital of Sakhalin Oblast, in the Russian Far East, with a population of around 173,000. Photo: Alkhimov Maxim, CC BY-SA 4.0. Photo: Wikimedia, CC BY-SA 2.0. Photo: Maarten, CC BY 2.0. Ukraine is facing shortages in its brave ...
Harris Chooses Walz
A guide to the career, politics and sudden stardom of Gov. Tim Walz of Minnesota, now Vice President Kamala Harris's running mate.